NDLI: Ternary invariant point at 403 and 455 °C in the Al–Sb

Content Provider	Springer Nature Link
Author	Klančnik, Grega Medved, Jožef
Copyright Year	2012
Abstract	The temperature and location of the invariant eutectic point at 403 °C in the zinc-rich corner of the Al–Sb–Zn system was determined. However, the experimentally determined temperature was found to be lower than the thermodynamically predicted one. Differential thermal analyses, differential scanning calorimetry, and quantitative microstructural analyses were used to determine this specific reaction. The determined ternary eutectic reaction, L → α-Sb$_{2}$Zn$_{3}$ + AlSb + η-Zn, represents the last solidification path in the phase region of Sb–AlSb–Zn. Before a ternary eutectic reaction takes place, another reaction is also possible near the Sb–Zn binary system, a quasi-peritectic reaction at 455 °C: L + β-Sb$_{2}$Zn$_{3}$ → AlSb + α-Sb$_{2}$Zn$_{3}$. A scanning electron microscope equipped with an energy-dispersive spectrometer was used for the microstructural analyses. The phase identification was conducted with X-ray diffractometry. The experimental data were compared to the thermodynamic predictions made with the CALPHAD method using the SSOL4 database.
Starting Page	243
Ending Page	248
Page Count	6
File Format	PDF
ISSN	13886150
Journal	Journal of thermal analysis
Volume Number	110
Issue Number	1
e-ISSN	15728943
Language	English
Publisher	Springer Netherlands
Publisher Date	2012-02-15
Publisher Place	Dordrecht
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	Thermal analysis Al–Sb–Zn ternary system Lead-free alloys Thermodynamic Measurement Science and Instrumentation Inorganic Chemistry Physical Chemistry Polymer Sciences Analytical Chemistry
Content Type	Text
Resource Type	Article
Subject	Physical and Theoretical Chemistry Condensed Matter Physics

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