NDLI: Sol–gel synthesis of 3-(triethoxysilyl)propylsuccinicanhydride containing fluorinated silane for hydrophobic surface applications

Content Provider	Springer Nature Link
Author	Kiraz, Nadir Burunkaya, Esin Kesmez, Ömer Asiltürk, Meltem Erdem Çamurlu, H. Arpaç, Ertuğrul
Copyright Year	2010
Abstract	In this paper, novel fluorinated silane compound was prepared by adding hydroxyl terminated Fluorolink D10H oligomer to 3-(triethoxysilyl)propylsuccinicanhydride. The obtained silane system was independently composed with 3-Aminopropyltrimethoxysilane, 3-Glycidyloxypropyltrimethoxysilane and 3-Glycidyloxypropyltriethoxysilane and, then the prepared coating solutions were applied to glass surface by spin-coating method. The chemical bonding between groups in system was investigated by Fourier Transform Infrared Spectroscopy analyses. The elemental composition of coatings was determined using Energy Dispersive X-ray Spectroscopy analyses. Its structure and surface properties were analyzed by scanning electron microscopy, atomic force microscopy, contact angle measurement and Ultraviolet–visible Absorption Spectroscopy. The amounts of fluorine on the coatings prepared with GF20-D10H-AMMO, GF20-D10H-GLYEO and GF20-D10H-GLYMO are 31, 32 and 34% at, respectively. Transparent coatings with smooth surface and uniform thickness were observed. The coatings had nanoscale roughness. The contact angles of coatings for water ranged from 88 to 107$^{o}$, and that of n-hexadecane ranged from 53 to 60$^{o}$.
Starting Page	157
Ending Page	166
Page Count	10
File Format	PDF
ISSN	09280707
Journal	Journal of Sol-Gel Science and Technology
Volume Number	56
Issue Number	2
e-ISSN	15734846
Language	English
Publisher	Springer US
Publisher Date	2010-07-21
Publisher Place	Boston
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	Fluorinated silane Sol–gel Hydrophobicity Oleophobicity Transparent coatings Nanotechnology Optical and Electronic Materials Inorganic Chemistry Ceramics, Glass, Composites, Natural Methods
Content Type	Text
Resource Type	Article
Subject	Ceramics and Composites Chemistry Materials Chemistry Biomaterials Condensed Matter Physics Electronic, Optical and Magnetic Materials

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