NDLI: Synthesis and characterisation of elastomeric composites prepared from epoxidised styrene butadiene rubber, 3-aminopropyltriethoxysilane and tetraethoxysilane

Content Provider	Springer Nature Link
Author	Luca, Maria Augusta Jacobi, Marly Maldaner Orlandini, Lisia Floriani
Copyright Year	2008
Abstract	Hybrid composite materials were obtained by the reaction of epoxidised styrene butadiene rubber with 3-aminopropyltriethoxysilane, followed by in situ hydrolysis and polycondensation of tetraethoxysilane (TEOS). The hybrid films were characterised by thermogravimetric analysis, differential scanning calorimetry, swelling and stress–strain measurements, scanning electron microscopy and infrared spectrometry. Non-solubility of the films in tetrahydrofuran indicated the formation of a network, the microstructure of which varied according to the concentrations of the inorganic precursors employed. The thermal stabilities of the films were similar to that of rubber, and the mechanical stress increased considerably with the amount of silica incorporated. The most transparent films were those prepared with the lowest concentrations of inorganic precursors, whilst those obtained using larger amounts of TEOS showed distinct microscopic phases. The protocol described represents a simple method by which to bind inorganic precursors to rubbers.
Starting Page	150
Ending Page	158
Page Count	9
File Format	PDF
ISSN	09280707
Journal	Journal of Sol-Gel Science and Technology
Volume Number	49
Issue Number	2
e-ISSN	15734846
Language	English
Publisher	Springer US
Publisher Date	2008-11-14
Publisher Place	Boston
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	Epoxidised rubber Silica Nanocomposites Tetraethoxysilane 3-Aminopropyltriethoxysilane Nanotechnology Optical and Electronic Materials Inorganic Chemistry Ceramics, Glass, Composites, Natural Methods
Content Type	Text
Resource Type	Article
Subject	Ceramics and Composites Chemistry Materials Chemistry Biomaterials Condensed Matter Physics Electronic, Optical and Magnetic Materials

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