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| Content Provider | Springer Nature Link |
|---|---|
| Author | Maxwell, S. L. Culligan, B. K. |
| Copyright Year | 2008 |
| Abstract | The Savannah River Site Environmental Bioassay Lab participated in the 2007 NRIP Emergency Response program administered by the National Institute for Standards and Technology (NIST) in May, 2007. A new rapid column separation method was applied directly to the NRIP 2007 emergency urine samples, with only minimal sample preparation to reduce preparation time. Calcium phosphate precipitation, used to preconcentrate actinides and $^{90}$Sr in NRIP 2006 urine and water samples, was not used for the NRIP 2007 urine samples. Instead, the raw urine was acidified and passed directly through the stacked resin columns (TEVA+TRU+SR-Resins) to separate the actinides and $^{90}$Sr from the NRIP urine samples more quickly. This improvement reduced sample preparation time for the NRIP 2007 emergency urine analyses significantly. This approach works well for small volume urine samples expected during an emergency response event. Based on initial feedback from NIST, the SRS Environmental Bioassay Lab had the most rapid analysis times for actinides and $^{90}$Sr analyses for NRIP 2007 emergency urine samples. |
| Starting Page | 105 |
| Ending Page | 111 |
| Page Count | 7 |
| File Format | |
| ISSN | 02365731 |
| Journal | Journal of Radioanalytical and Nuclear Chemistry |
| Volume Number | 279 |
| Issue Number | 1 |
| e-ISSN | 15882780 |
| Language | English |
| Publisher | Springer Netherlands |
| Publisher Date | 2008-07-21 |
| Publisher Place | Dordrecht |
| Access Restriction | One Nation One Subscription (ONOS) |
| Subject Keyword | Inorganic Chemistry Diagnostic Radiology Nuclear Physics, Heavy Ions, Hadrons Physical Chemistry Nuclear Chemistry |
| Content Type | Text |
| Resource Type | Article |
| Subject | Spectroscopy Pollution Health, Toxicology and Mutagenesis Radiology, Nuclear Medicine and Imaging Analytical Chemistry Public Health, Environmental and Occupational Health Nuclear Energy and Engineering |
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