NDLI: A Novel Approach for the Synthesis and Characterization Studies of Mn $^{ 2 + }$-Doped CdS Nanocrystals by a Facile Microwave-Assisted Combustion Method

Content Provider	Springer Nature Link
Author	Manikandan, A. Antony, S. Arul
Copyright Year	2014
Abstract	A simple and efficient microwave-assisted combustion method was developed to synthesize Mn $^{2+}$-doped CdS (Mn $_{ x }$Cd $_{1−x}$S: x= 0.0, 0.3, and 0.5) nanocrystallites. The study suggested that the application of microwave heating produced spherical shaped cluster of pure and Mn $^{2+}$-doped CdS nanocrystallites, which was achieved in few minutes. The effects of Mn $^{2+}$-doping on structural, morphological, optical and magnetic properties of CdS nanocrystallites were investigated by powder X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FT-IR), high-resolution scanning electron microscopy (HR-SEM) with energy dispersive X-ray analysis (EDX), high-resolution transmission electron microscopy (HR-TEM) with selected area electron diffraction (SAED), UV-Visible diffuse reflectance spectroscopy (DRS), photoluminescence (PL) spectroscopy, and vibrating sample magnetometer (VSM). The XRD results confirmed the formation of hexagonal CdS. The formation of pure and Mn $^{2+}$-doped CdS phase was also confirmed by FT-IR and EDX. The formation of spherical shaped cluster of nanocrystallites was confirmed by HR-SEM and HR-TEM. The as-synthesized nanocrystallites were found to have good optoelectronic properties that were determined by DRS and PL spectra. VSM results of the as-synthesized Mn $^{2+}$-doped CdS nanocrystallites showed ferromagnetic behavior. Graphical Abstract A simple and rapid microwave-assisted combustion method was developed to synthesize pure and Mn2+-doped CdS-nanocrystallites. The formation of spherical shaped cluster of nano-crystallites was confirmed by HR-SEM and HR-TEM. The optical properties were determined by DRS and PL spectra. Magnetic properties were analyzed by VSM.
Starting Page	2725
Ending Page	2733
Page Count	9
File Format	PDF
ISSN	15571939
Journal	Journal of Superconductivity and Novel Magnetism
Volume Number	27
Issue Number	12
e-ISSN	15571947
Language	English
Publisher	Springer US
Publisher Date	2014-09-03
Publisher Place	New York
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	CdS nanocrystals Combustion method Electron microscopy Magnetic properties Optical properties X-ray diffraction Strongly Correlated Systems, Superconductivity Magnetism, Magnetic Materials Condensed Matter Physics Characterization and Evaluation of Materials
Content Type	Text
Resource Type	Article
Subject	Electronic, Optical and Magnetic Materials Condensed Matter Physics

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