NDLI: Spectroscopy of extended electron energy loss fine structures for quantitative analysis of the local atomic structure in ultrathin oxide films on the surface of 3d-metals

Content Provider	Springer Nature Link
Author	Gai, D. E. Grebennikov, V. I. Bakieva, O. R. Surnin, D. V. Deev, A. N.
Copyright Year	2008
Abstract	The work presents the theoretical description of formation processes of extended electron energy loss fine structure (EELFS) spectra. Simple analytical formulas are obtained to calculate EELFS spectra. Methods are proposed to compute amplitudes and intensities of electronic transitions of different multipolarity in electron-impact excitation of the inner shell of an atom. The corresponding test calculations are performed. We present experimental M $_{2,3}$ EELFS spectra of 3d-metals obtained from clean surfaces of Fe, Ni, and Cu and ultrathin stoichiometric oxide films of Fe$_{2}$O$_{3}$, NiO, and CuO as well as K EELFS spectra of oxygen from thin stoichiometric oxide films. Techniques are proposed to extract normalized oscillating parts from experimental EELFS data based on the use of calculated intensities of the corresponding electronic transitions. Atomic pair correlation functions are obtained for the objects under study from experimental EELFS data with regard to multipolarity of electron impact excitation of the atomic inner shell. Experimental results correspond well to known crystallographic data (partial interatomic distances, coordination numbers, and Debye-Waller factors).
Starting Page	174
Ending Page	189
Page Count	16
File Format	PDF
ISSN	00224766
Journal	Journal of Structural Chemistry
Volume Number	49
Issue Number	1
e-ISSN	15738779
Language	English
Publisher	Springer US
Publisher Date	2009-03-15
Publisher Place	Boston
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	scattering theory atomic pair correlation functions electron energy loss spectroscopy ultrathin oxide films Solid State Physics and Spectroscopy Atomic and Molecular Structure and Spectra Atoms, Molecules, Clusters and Plasmas Physical Chemistry Inorganic Chemistry
Content Type	Text
Resource Type	Article
Subject	Materials Chemistry Physical and Theoretical Chemistry Inorganic Chemistry

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