NDLI: Synthesis and Characterisation of Polyester Based on Isosorbide and Butanedioic Acid

Content Provider	Springer Nature Link
Author	Ristić, Ivan S. Vukić, Nevena Cakić, Suzana Simendić, Vesna Ristić, Olivera Budinski Simendić, Jaroslava
Copyright Year	2012
Abstract	Copolyesters based on isosorbide and butanedioic acid in combination with monomers such as adipic acid and dimethyl terephthalate, poly(isosorbide-co-butanedioic acid) (and -co-adipic acid) and poly(isosorbide-co-butanedioic acid-co-dimethyl terephthalate), were synthesized and characterized. Linear OH-functionalized polyesters were obtained via melt polyesterification of dicarboxylic acids with OH-functional monomers. The type of end-group was controlled by the monomer stoichiometry and hydroxyl functional group is formed in time. Average molecular masses of synthesised polyesters were measured by gel permeation chromatography. The glass transition temperatures and thermal stability of the obtained polyesters were effectively adjusted by varying polymer composition and molar mass. Addition of adipic acid or dimethyl terephthalate increased glass transition temperatures of obtained polyesters. Thermal stability of obtained polyester slightly increases by the increasing of dimethyl terephthalate content. Molecular structures of obtained polyester were assessed by Fourier transform infrared spectra and $^{1}$H NMR spectroscopy.
Starting Page	519
Ending Page	527
Page Count	9
File Format	PDF
ISSN	15662543
Journal	Journal of Polymers and the Environment
Volume Number	20
Issue Number	2
e-ISSN	15728900
Language	English
Publisher	Springer US
Publisher Date	2012-01-18
Publisher Place	Boston
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	Biobased polyester Isosorbide $^{1}$H NMR Thermal properties Polymer Sciences
Content Type	Text
Resource Type	Article
Subject	Materials Chemistry Environmental Engineering Polymers and Plastics

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