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Microwave Assisted Synthesis of Bio Based Metallopolyurethaneamide

Content Provider	Springer Nature Link
Author	Zafar, Fahmina Mir, Muzaffar Hassan Kashif, Mohammad Sharmin, Eram Ahmad, Sharif
Copyright Year	2010
Abstract	In the present work, microwave assisted synthesis of metallopolyurethaneamide (MicMCPUA) has been carried out from Castor seed oil. The aim of the work is (i) to utilize non toxic, abundantly available bioresources—seed oils, (ii) to develop environment friendly metallopolymers, as vital alternate to petrobased materials, (iii) through “green” technology-microwave assisted synthesis, for the first time, (iv) for application as ecofriendly protective coatings. MicMCPUA was synthesized “in situ” under microwave irradiations by the reaction of microwave assisted diol Castor fattyamide (MicDCFA, as organic matrix) and zinc acetates (5, 10 and 15 wt%, as inorganic modifier) without any harmful solvents resulting in the formation of pre-metallopolymer (MicMDCFA) that was further reacted with toluylene-2,4-diisocyanate (TDI). The effect of metal incorporation on structural (spectral), physico-chemical and thermal stability of metallopolyurethaneamide was studied by standard methods. The coating performance of the metallopolyurethaneamide was also investigated by physico-mechanical and potentiodynamic polarization measurements. These studies revealed that MicMCPUA may find application as eco-friendly corrosion protective coatings safely up to 200–220 °C.
Starting Page	61
Ending Page	68
Page Count	8
File Format	PDF
ISSN	15741443
Journal	Journal of Inorganic and Organometallic Polymers and Materials
Volume Number	21
Issue Number	1
e-ISSN	15741451
Language	English
Publisher	Springer US
Publisher Date	2010-10-19
Publisher Place	Boston
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	Microwave assisted Castor oil Metallopolyurethaneamide TGA FTIR Potentiodynamic polarization Polymer Sciences Organic Chemistry Inorganic Chemistry
Content Type	Text
Resource Type	Article
Subject	Materials Chemistry Polymers and Plastics

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