NDLI: Zn$_{x}$Cu$_{(1−x)}$Fe$_{2}$O$_{4}$ Nanoferrites by Sol–Gel Auto Combustion Route: Cation Distribution and Microwave Absorption Properties

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Zn$_{x}$Cu$_{(1−x)}$Fe$_{2}$O$_{4}$ Nanoferrites by Sol–Gel Auto Combustion Route: Cation Distribution and Microwave Absorption Properties

Content Provider	Springer Nature Link
Author	Kavas, H. Baykal, A. Demir, A. Toprak, M. S. Aktaş, B.
Copyright Year	2014
Abstract	The effect of Zn doping on magnetic properties and site preference of cations of CuFe$_{2}$O$_{4}$ has been investigated. Zn substituted Cu ferrite nanoparticles with general formula Zn$_{x}$Cu$_{(1−x)}$Fe$_{2}$O$_{4}$ were synthesized by a sol–gel auto combustion method. Samples showed fine particle size with very strong aggregation, due to the high temperatures attained during the combustion process. All samples showed high phase purity assessed from X-ray diffraction analysis and do not have magnetization hysteresis, which reveals superparamagnetic character of the fabricated particles. It was found that a certain amount of Zn substitution in Cu ferrite (0.4 < x < 0.6) causes different site occupation of cations. XRD and magnetic hysteresis data of all samples were analyzed and the cation distribution in spinel ferrites was calculated by these two experimental techniques. It was found that the Neel antiferromagnetic aligned sublattice model is valid below this region (x < 0.4), and above it (x > 0.6) the canted spins at octahedral site are dominant according to the tetrahedral site spins.
Starting Page	963
Ending Page	970
Page Count	8
File Format	PDF
ISSN	15741443
Journal	Journal of Inorganic and Organometallic Polymers and Materials
Volume Number	24
Issue Number	6
e-ISSN	15741451
Language	English
Publisher	Springer US
Publisher Date	2014-09-06
Publisher Place	Boston
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	Magnetic materials Reflection loss Cation distribution Permittivity Permeability Inorganic Chemistry Organic Chemistry Polymer Sciences
Content Type	Text
Resource Type	Article
Subject	Materials Chemistry Polymers and Plastics

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