NDLI: An investigation on the properties of SnO$_{2}$ nanoparticles synthesized using two different methods

Content Provider	Springer Nature Link
Author	Shalan, A. E. Osama, I. Rashad, M. M. Ibrahim, I. A.
Copyright Year	2013
Abstract	Tin oxide SnO$_{2}$ nanoparticles have been synthesized using chemical co-precipitation and solvothermal methods. The structures and morphologies of SnO$_{2}$ prepared using both routes were characterized using X-ray diffraction (XRD), transmission electron microscopy (TEM), fourier infrared absorption spectroscopy (FT-IR), UV–Vis Spectroscopy and BET specific surface area. The XRD patterns showed the presence of the tetragonal structure in the nanometric range and both crystallinity as well as crystal size increased with the increasing in temperature. The size of the produced tin dioxide nanoparticles was from 6.2 to 10.6 nm by solvothermal route while it was from 9.3 to 16.2 nm for nanoparticles by co-precipitation pathway. Furthermore, TEM results showed that the sizes of SnO$_{2}$ particles in all powders were tetragonal like structure and the grain size was increased with temperature. FT-IR spectra revealed that intensity of the transverse optical mode of Sn–O stretching vibration was increased with the sintering temperature while the bending vibration of O–Sn–O showed a blue shift. The optical band gap was shifted to a lower energy with increasing temperature due to the improvement of the crystallinity and the value was varied from 2.9 to 4.25 eV. The specific surface area of the as-made SnO$_{2}$ in comparison with such calcined samples decreased with increasing the calcination temperature due to the changes in the sample particle size and in the sample crystal phases.
Starting Page	303
Ending Page	310
Page Count	8
File Format	PDF
ISSN	09574522
Journal	Journal of Materials Science: Materials in Electronics
Volume Number	25
Issue Number	1
e-ISSN	1573482X
Language	English
Publisher	Springer US
Publisher Date	2013-11-07
Publisher Place	Boston
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	Optical and Electronic Materials Characterization and Evaluation of Materials
Content Type	Text
Resource Type	Article
Subject	Atomic and Molecular Physics, and Optics Biomaterials Biophysics Condensed Matter Physics Electronic, Optical and Magnetic Materials Bioengineering Electrical and Electronic Engineering Biomedical Engineering

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