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| Content Provider | Springer Nature Link |
|---|---|
| Author | Sayed Abhudhahir, Mohammed Harshulkhan Kandasamy, Janaki |
| Copyright Year | 2015 |
| Abstract | The aim of this article is to prepare Tungsten oxide (WO$_{3}$) nanoparticle along with manganese (3 and 10 wt%) by Microwave irradiation method. The physical properties of the synthesized Mn doped WO$_{3}$ materials were characterized by X-ray diffraction (XRD), Fourier transform infra-red spectroscopy (FTIR), transmission electron microscope (TEM), UV-diffuse reflectance spectroscopy and photoluminescence studies. Powder XRD results reveal that the Mn doped WO$_{3}$ crystallizes in monoclinic structure. FTIR spectroscopy analysis reveals the presence of tungsten and oxygen in the synthesised material. TEM micrograph illustrate that both pristine and Mn doped WO$_{3}$ nanopaticles are having spherical shaped morphology with average particle size from 35–50 nm. A significant red shift in the absorption edge and decrease the band gap energy for WO$_{3}$ nanoparticles were confirmed with UV-DRS spectra analysis. The defects and oxygen deficiencies were analysed by photoluminescence spectroscopy. The photocatalytic activites of the pure and Mn doped WO$_{3}$ samples were evaluated by the degradation of methylene blue in a aqueous solution under visible light irradiation. The photocatalytic activity for Mn doped WO$_{3}$ was much higher than that of the pure WO$_{3}$. |
| Starting Page | 8307 |
| Ending Page | 8314 |
| Page Count | 8 |
| File Format | |
| ISSN | 09574522 |
| Journal | Journal of Materials Science: Materials in Electronics |
| Volume Number | 26 |
| Issue Number | 11 |
| e-ISSN | 1573482X |
| Language | English |
| Publisher | Springer US |
| Publisher Date | 2015-07-23 |
| Publisher Place | New York |
| Access Restriction | One Nation One Subscription (ONOS) |
| Subject Keyword | Optical and Electronic Materials Characterization and Evaluation of Materials |
| Content Type | Text |
| Resource Type | Article |
| Subject | Atomic and Molecular Physics, and Optics Biomaterials Biophysics Condensed Matter Physics Electronic, Optical and Magnetic Materials Bioengineering Electrical and Electronic Engineering Biomedical Engineering |
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