NDLI: A simple synthesis of amine-derivatised superparamagnetic iron oxide nanoparticles for bioapplications

Content Provider	Springer Nature Link
Author	Mohapatra, Sasmita Pramanik, Nabakumar Mukherjee, Samrat Ghosh, Sudip K. Pramanik, Panchanan
Copyright Year	2007
Abstract	Adsorption of 3-aminopropyltriethoxysilane (APTS) on magnetite nanoparticles during its formation has been investigated to optimise the preparation of stable aqueous dispersion of amine derivatised magnetite nanoparticles. APTS adsorbs chemically on the surface of magnetite particle modifying its surface which is evident from thermal and C, H, N analysis. The variation of particle size has been observed with change of APTS concentration. X-ray diffractogram shows the formation of pure inverse spinel phase magnetite with average crystallite size 7 nm when equimolar (Fe$_{3}$O$_{4}$: APTS = 1:1) quantity of APTS was used during its synthesis. The presence of free surface –NH$_{2}$ groups and Fe–O–Si bonds was observed by FTIR. Raman spectrum further confirms the presence of surface –NH$_{2}$ groups. Transmission electron microscopy shows formation of particles of average size between 7 nm and 12 nm. The effective hydrodynamic diameter of the APTS coated particle agglomerates is 45.8 nm in stable aqueous colloidal dispersion, which is evident from photon correlation spectroscopy. VSM measurements at room temperature of both silanised and unsilanised magnetite shows their superparamagnetic nature with saturation magnetisation 41 e.m.u/g and 56 e.m.u/g, respectively. Avidin has been immobilised on the surface through glutaraldehyde, which demonstrates the possibility of the synthesised material to be used in protein immobilisation to form bioactive magnetic particles.
Starting Page	7566
Ending Page	7574
Page Count	9
File Format	PDF
ISSN	00222461
Journal	Journal of Materials Science
Volume Number	42
Issue Number	17
e-ISSN	15734803
Language	English
Publisher	Kluwer Academic Publishers-Plenum Publishers
Publisher Date	2007-05-24
Publisher Place	New York
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	Mechanics Crystallography Continuum Mechanics and Mechanics of Materials Polymer Sciences Characterization and Evaluation of Materials Materials Science
Content Type	Text
Resource Type	Article
Subject	Ceramics and Composites Mechanics of Materials Mechanical Engineering Polymers and Plastics

Sl.	Authority	Responsibilities	Communication Details
1	Ministry of Education (GoI), Department of Higher Education	Sanctioning Authority	https://www.education.gov.in/ict-initiatives
2	Indian Institute of Technology Kharagpur	Host Institute of the Project: The host institute of the project is responsible for providing infrastructure support and hosting the project	https://www.iitkgp.ac.in
3	National Digital Library of India Office, Indian Institute of Technology Kharagpur	The administrative and infrastructural headquarters of the project	Dr. B. Sutradhar bsutra@ndl.gov.in
4	Project PI / Joint PI	Principal Investigator and Joint Principal Investigators of the project	Dr. B. Sutradhar bsutra@ndl.gov.in Prof. Saswat Chakrabarti will be added soon
5	Website/Portal (Helpdesk)	Queries regarding NDLI and its services	support@ndl.gov.in
6	Contents and Copyright Issues	Queries related to content curation and copyright issues	content@ndl.gov.in
7	National Digital Library of India Club (NDLI Club)	Queries related to NDLI Club formation, support, user awareness program, seminar/symposium, collaboration, social media, promotion, and outreach	clubsupport@ndl.gov.in
8	Digital Preservation Centre (DPC)	Assistance with digitizing and archiving copyright-free printed books	dpc@ndl.gov.in
9	IDR Setup or Support	Queries related to establishment and support of Institutional Digital Repository (IDR) and IDR workshops	idr@ndl.gov.in

Synthesis and characterization of iron oxide nanoparticles dispersed in mesoporous aluminum oxide or silicon oxide

Surface ligand influenced free radical protection of superparamagnetic iron oxide nanoparticles (SPIONs) toward H9c2 cardiac cells

Synthesis of tunable sized capped magnetic iron oxide nanoparticles highly soluble in organic solvents

Novel photoactive inorganic polymer composites of inorganic polymers with copper(I) oxide nanoparticles

Synthesis and characterization of iron-substituted hydroxyapatite via a simple ion-exchange procedure

The synthesis of graphene oxide nanostructures for supercapacitors: a simple route

TEM characterization of iron-oxide-coated ceramic membranes

AFM and SEM characterization of iron oxide coated ceramic membranes

Synthesis and characterization of layered and scrolled amine-templated vanadium oxides

A simple synthesis of amine-derivatised superparamagnetic iron oxide nanoparticles for bioapplications

Similar Documents

Synthesis and characterization of iron oxide nanoparticles dispersed in mesoporous aluminum oxide or silicon oxide

Surface ligand influenced free radical protection of superparamagnetic iron oxide nanoparticles (SPIONs) toward H9c2 cardiac cells

Synthesis of tunable sized capped magnetic iron oxide nanoparticles highly soluble in organic solvents

Novel photoactive inorganic polymer composites of inorganic polymers with copper(I) oxide nanoparticles

Synthesis and characterization of iron-substituted hydroxyapatite via a simple ion-exchange procedure

The synthesis of graphene oxide nanostructures for supercapacitors: a simple route

TEM characterization of iron-oxide-coated ceramic membranes

AFM and SEM characterization of iron oxide coated ceramic membranes

Synthesis and characterization of layered and scrolled amine-templated vanadium oxides

A simple synthesis of amine-derivatised superparamagnetic iron oxide nanoparticles for bioapplications