NDLI: Processing of composites in the Ti-Si-C system

Content Provider	Springer Nature Link
Author	Park, C. S. Zheng, F. Salamone, S. Bordia, R. K.
Copyright Year	2001
Abstract	New composites utilizing Ti$_{3}$SiC$_{2}$ as the matrix phase have been synthesized. The thermal and kinetic aspects of the phase formation in the Ti-Si-C system were examined. Standard dry powder processing techniques, pressureless sintering and hot pressing (both under inert atmosphere) were employed to process the sample materials. The phase identification was performed by X-ray powder diffraction (XRPD) analysis. The ratio of the volume fractions of the reinforcement phases SiC and/or TiC$_{ x }$ to the matrix phase Ti$_{3}$SiC$_{2}$ have been measured and tailored over a wide range by means of controlling the stoichiometry of the starting elemental powders and varying the heat treatment. It was found that the Si tends to evaporate at elevated temperatures during sintering. The loss of Si is the likely reason why it is difficult to form the single phase Ti$_{3}$SiC$_{2}$. Incorporating this observation into the composite formation, a method to form in-situ composites is proposed. The volume fraction of the constituent phase in the composite can be controlled by varying the processing parameters.
Starting Page	3313
Ending Page	3322
Page Count	10
File Format	PDF
ISSN	00222461
Journal	Journal of Materials Science
Volume Number	36
Issue Number	13
e-ISSN	15734803
Language	English
Publisher	Kluwer Academic Publishers
Publisher Date	2001-01-01
Publisher Place	Boston
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	Polymer Sciences Industrial Chemistry/Chemical Engineering Characterization and Evaluation Materials Mechanics
Content Type	Text
Resource Type	Article
Subject	Ceramics and Composites Mechanics of Materials Mechanical Engineering Polymers and Plastics

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