NDLI: Intercalation Compounds between Ethyl 2-oxocyclopentanecarboxylate and Saponite

Content Provider	Springer Nature Link
Author	Merchan, Nuria Angel Bañares Muñoz, Miguel Vicente, Miguel Angel
Copyright Year	1998
Abstract	The retention of ethyl 2-oxocyclopentanecarboxylate by a saponite has been studied. Intercalation compounds were prepared by two different methods: 1) in repose at room temperature and 2) heating at 60 °C under reflux. Contact times between 2 and 12 days were considered for each method. The intercalation compounds obtained were characterized by X-ray diffraction, infrared spectroscopy, chemical analyses and thermal analyses. This characterization indicates that the organic compound is retained both in the interlayer region and at the edge of the clay particles. The amount retained outside of the interlayer space is eliminated by careful washing with benzene and cyclohexane. The results obtained when using acid-activated saponite -obtained by treatment of the clay with dilute HCl solutions- in the intercalation experiments were similar to those obtained when using non-activated saponite.
Starting Page	219
Ending Page	230
Page Count	12
File Format	PDF
ISSN	09230750
Journal	Journal of Inclusion Phenomena and Macrocyclic Chemistry
Volume Number	31
Issue Number	3
e-ISSN	15731111
Language	English
Publisher	Kluwer Academic Publishers
Publisher Date	1998-01-01
Publisher Place	Dordrecht
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	Food Science Organic Chemistry Crystallography
Content Type	Text
Resource Type	Article
Subject	Chemistry Condensed Matter Physics Food Science

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