NDLI: The validity of commercial LIBS for quantitative analysis of brass alloy

Content Provider	Springer Nature Link
Author	Shaltout, Abdallah A. Abdel Aal, M. S. Mostafa, N. Y.
Copyright Year	2011
Abstract	Commercial low-cost laser induced breakdown spectroscopy (LIBS) has been successfully employed for the quantitative analysis of a Cu-based alloy using a Nd:YAG laser at 1064 nm. The main aim of the present investigation is to explore the benefits of a commercial low-cost LIBS setup. It was recognized that some trace elements such as Al and S could not be detected by LIBS even with a high-resolution spectrometer. The main difficulties in quantifying Cu as a basic component of a brass alloy are related to the self-absorption of Cu spectral lines, with the effect complicated at Cu concentrations higher than 65%. However, few Cu lines such as that at 330.795 nm would be helpful to use due to their lower susceptibility to self-absorption. LIBS, flame atomic absorption spectrometry (FAAS), and wavelength dispersive X-ray fluorescence (WDXRF) were compared for the detection of major and trace metals in the Cu-based alloy. In the case of WDXRF, the brass samples were identified by using a standardless quantitative analysis program depending on a fundamental parameter approach. The quantitative analysis results were acceptable for most of the major and minor elements of the brass sample. Therefore, commercial low cost LIBS would be useful for quantitative analysis of most elements in different types of alloys.
Starting Page	594
Ending Page	600
Page Count	7
File Format	PDF
ISSN	00219037
Journal	Journal of Applied Spectroscopy
Volume Number	78
Issue Number	4
e-ISSN	15738647
Language	English
Publisher	Springer US
Publisher Date	2011-09-17
Publisher Place	Boston
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	brass alloy laser-induced breakdown spectroscopy wavelength dispersive X-ray fluorescence atomic absorption spectrometry Atomic/Molecular Structure and Spectra Analytical Chemistry
Content Type	Text
Resource Type	Article
Subject	Spectroscopy Condensed Matter Physics

Sl.	Authority	Responsibilities	Communication Details
1	Ministry of Education (GoI), Department of Higher Education	Sanctioning Authority	https://www.education.gov.in/ict-initiatives
2	Indian Institute of Technology Kharagpur	Host Institute of the Project: The host institute of the project is responsible for providing infrastructure support and hosting the project	https://www.iitkgp.ac.in
3	National Digital Library of India Office, Indian Institute of Technology Kharagpur	The administrative and infrastructural headquarters of the project	Dr. B. Sutradhar bsutra@ndl.gov.in
4	Project PI / Joint PI	Principal Investigator and Joint Principal Investigators of the project	Dr. B. Sutradhar bsutra@ndl.gov.in Prof. Saswat Chakrabarti will be added soon
5	Website/Portal (Helpdesk)	Queries regarding NDLI and its services	support@ndl.gov.in
6	Contents and Copyright Issues	Queries related to content curation and copyright issues	content@ndl.gov.in
7	National Digital Library of India Club (NDLI Club)	Queries related to NDLI Club formation, support, user awareness program, seminar/symposium, collaboration, social media, promotion, and outreach	clubsupport@ndl.gov.in
8	Digital Preservation Centre (DPC)	Assistance with digitizing and archiving copyright-free printed books	dpc@ndl.gov.in
9	IDR Setup or Support	Queries related to establishment and support of Institutional Digital Repository (IDR) and IDR workshops	idr@ndl.gov.in

Investigation of Pb in Gannan Navel Orange with Contaminant in Controlled Conditions by Laser-Induced Breakdown Spectroscopy

Assessment of metal elements in final drug products by wavelength dispersive X-ray fluorescence spectrometry

Evaluation of Detection Limits with Wavelength Dispersive X-Ray Fluorescence Spectrometry

Evaluation of Detection Limits with Wavelength Dispersive X-Ray Fluorescence Spectrometry

Evaluation of Detection Limits with Wavelength Dispersive X-Ray Fluorescence Spectrometry

Optimization of a Laser Induced Breakdown Spectroscopy Method for the Analysis of Liquid Samples

Application and Validation of Analytical Software (SQX) for Semi-Quantitative Determination of the Main Chemical Composition of Solid, Bulk and Powder Fuel Samples by Wavelength Dispersive X-ray Fluorescence Technique

Nuclear Microscopy for Air-Pollutant Characterization and Its Advantages over Traditional Techniques

Multi-element analysis of soils and sediments by wavelength-dispersive X-ray fluorescence spectrometry

The validity of commercial LIBS for quantitative analysis of brass alloy — comparison of WDXRF and AAS

Similar Documents

Investigation of Pb in Gannan Navel Orange with Contaminant in Controlled Conditions by Laser-Induced Breakdown Spectroscopy

Assessment of metal elements in final drug products by wavelength dispersive X-ray fluorescence spectrometry

Evaluation of Detection Limits with Wavelength Dispersive X-Ray Fluorescence Spectrometry

Evaluation of Detection Limits with Wavelength Dispersive X-Ray Fluorescence Spectrometry

Evaluation of Detection Limits with Wavelength Dispersive X-Ray Fluorescence Spectrometry

Optimization of a Laser Induced Breakdown Spectroscopy Method for the Analysis of Liquid Samples

Application and Validation of Analytical Software (SQX) for Semi-Quantitative Determination of the Main Chemical Composition of Solid, Bulk and Powder Fuel Samples by Wavelength Dispersive X-ray Fluorescence Technique

Nuclear Microscopy for Air-Pollutant Characterization and Its Advantages over Traditional Techniques

Multi-element analysis of soils and sediments by wavelength-dispersive X-ray fluorescence spectrometry

The validity of commercial LIBS for quantitative analysis of brass alloy — comparison of WDXRF and AAS