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Functionalized SBA-15 and its Catalytic Applications in Selective Organic Transformations

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Functionalized SBA-15 and its Catalytic Applications in Selective Organic Transformations

Content Provider	Springer Nature Link
Author	Srinivas, Darbha Saikia, Lakshi
Copyright Year	2008
Abstract	Ordered, mesoporous SBA-15 functionalized with organic and inorganic moieties exhibits efficient catalytic activity in a variety of organic transformations. In this account, reviewing our own work, three-sets of surface-modified SBA-15 materials have been investigated. The first-set of materials consists of SBA-15 modified with organo-acidic (propyl thiol and propyl sulfonic acid) and basic (propyl amine and propyl adenine) moieties. The second-set of materials was prepared by grafting Mn complexes to the organo-functionalized SBA-15. The third-set composes of nanocrystalline metal oxides supported on SBA-15. All these catalysts have been characterized by structural and spectroscopic techniques. Catalytic activities of the first-set of solid materials have been investigated in acid/base-catalyzed reactions viz., ring-opening of epoxides with amines (producing β-amino alcohols), esterification, three-component-Mannich reactions and cycloaddition of CO2 to epoxides. The Mn complexes grafted on organofunctionalized SBA-15 are efficient catalysts for the chemo-, regio- and stereoselective aerial oxidation of monoterpenes at ambient conditions. TiOx, VOx, MoOx and WOx supported on SBA-15 catalyzed biomimetic oxyhalogenation of aromatic compounds. In all these reactions, the functionalized SBA-15 showed high selectivity.
Starting Page	114
Ending Page	130
Page Count	17
File Format	PDF
ISSN	15711013
Journal	Catalysis Surveys from Asia
Volume Number	12
Issue Number	2
e-ISSN	15749266
Language	English
Publisher	Springer US
Publisher Date	2008-04-30
Publisher Place	Boston
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	Ordered mesoporous silica Organofunctionalized SBA-15 Grafted Mn–Salen complexes Oxidation catalysts Oxyhalogenation of aromatics Characterization and Evaluation of Materials Industrial Chemistry/Chemical Engineering Physical Chemistry Catalysis
Content Type	Text
Resource Type	Article
Subject	Chemistry Catalysis

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