NDLI: Determination of BTEX Compounds in Solid–Liquid Mixing Paint Using the Combination of Solid Phase Extraction, Thermal Desorption and GC-FID

Content Provider	Springer Nature Link
Author	Zhang, Shuai Zhao, Tianbo Xu, Xin Wang, Haiwang Miao, Ce
Copyright Year	2010
Abstract	A novel method was developed and validated for determination of benzene, toluene, p-xylene, m-xylene, o-xylene (BTEX) in a solid–liquid mixing matrix. It makes use of solid phase extraction and thermal desorption (SPE-TD), followed by gas chromatographic flame ionization detector analysis (GC-FID). The trapped BTEX can be measured directly after thermal desorption onto the stainless-steel packed chromatographic column. The effect of tailing area of solvent was removed with the use of SPE-TD technique, and the result shows good reproducibility with very little matrix dependency. The study also supports that the lifetime of the Tenax adsorption tube could be extended over 150 desorption operation at 200 °C, which enables performing excellent stability and reproducibility of BTEX analysis.
Starting Page	1131
Ending Page	1135
Page Count	5
File Format	PDF
ISSN	00095893
Journal	Chromatographia
Volume Number	71
Issue Number	11-12
e-ISSN	16121112
Language	English
Publisher	Vieweg Verlag
Publisher Date	2010-04-20
Publisher Place	Wiesbaden
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	Gas chromatography Solid phase extraction and thermal desorption Stainless-steel packed chromatographic column BTEX in painting materials Measurement Science and Instrumentation Plant Sciences Biochemistry Pharmacy Organic Chemistry Analytical Chemistry
Content Type	Text
Resource Type	Article
Subject	Organic Chemistry Analytical Chemistry Biochemistry Clinical Biochemistry

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