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| Content Provider | Springer Nature Link |
|---|---|
| Author | Chen, Zilei Zhang, Hong Liu, Bing Yang, Guosheng Aboul Enein, Hassan Y. Wang, Wenbo Ding, Ruiyan Du, Hongxia Li, Huidong |
| Copyright Year | 2007 |
| Abstract | A rapid multi-residue method has been developed for the determination of 16 herbicides in garlic. The analytical procedure is based on prior microwave heating prevention of the generation of sulfur-containing compounds. The garlic samples which had been pretreated were extracted with acetonitrile and cleaned up by solid-phase extraction. The herbicide residues were detected by gas chromatography–mass spectrometry with selected ion monitoring. The recoveries of 16 herbicides ranged from 69.0 to 105.4% with the relative standard deviations (RSD) below 10.1%. The limit of quantification (LOQ) ranged from 0.003 to 0.015 mg kg−1. |
| Starting Page | 887 |
| Ending Page | 891 |
| Page Count | 5 |
| File Format | |
| ISSN | 00095893 |
| Journal | Chromatographia |
| Volume Number | 66 |
| Issue Number | 11-12 |
| e-ISSN | 16121112 |
| Language | English |
| Publisher | Vieweg Verlag |
| Publisher Date | 2007-10-19 |
| Publisher Place | Wiesbaden |
| Access Restriction | One Nation One Subscription (ONOS) |
| Subject Keyword | Gas chromatography–mass spectrometry Microwave sulfur removal Garlic Herbicide residues Measurement Science, Instrumentation Plant Sciences Biochemistry Pharmacy Organic Chemistry Analytical Chemistry |
| Content Type | Text |
| Resource Type | Article |
| Subject | Organic Chemistry Analytical Chemistry Biochemistry Clinical Biochemistry |
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