NDLI: Multi-Residue Analysis of 205 Crop Pesticides Using Mini-Solid Phase Extraction–Large Volume Injection–GC

Content Provider	Springer Nature Link
Author	Xu, Xiu Li Li, Li Zhong, Wei Ke He, Yu Jian
Copyright Year	2009
Abstract	A simple, rapid, and sensitive multi-residue method has been developed for the determination of 205 pesticides commonly used for crop protection. Pesticide residues were extracted from samples with acetonitrile and a mini-solid phase extraction filter. No additional concentration or clean-up steps were necessary. Analyses were performed via large volume gas chromatography injection using a stomach-shaped inlet liner. The developed method was linear over the range assayed (5–50 μg L−1), with determination coefficients >0.99. The limits of quantification were in the range 0.0005–0.6 mg kg−1 and the limits of detection were between 0.00015 and 0.2 mg kg−1. The majorities of them were lower than the maximum residue set by the Japanese government in “Positive System for Agricultural Chemical Residues in Food” directive in apple. This method was applied to determine pesticide levels in vegetables, fruits, and beans.
Starting Page	173
Ending Page	183
Page Count	11
File Format	PDF
ISSN	00095893
Journal	Chromatographia
Volume Number	70
Issue Number	1-2
e-ISSN	16121112
Language	English
Publisher	Vieweg Verlag
Publisher Date	2009-05-22
Publisher Place	Wiesbaden
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	Gas chromatography–mass spectrometry Mini-solid phase extraction Multi-residue methods Large volume injection Pesticides Measurement Science, Instrumentation Plant Sciences Biochemistry Pharmacy Organic Chemistry Analytical Chemistry
Content Type	Text
Resource Type	Article
Subject	Organic Chemistry Analytical Chemistry Biochemistry Clinical Biochemistry

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