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| Content Provider | Springer Nature Link |
|---|---|
| Author | Choi, Hoon Park, Sung Kug Kim, Dong Sul Kim, Meehye |
| Copyright Year | 2011 |
| Abstract | The analytical method was developed for the speciation of 6 arsenic species [As(III), As(V), monomethylarsonic acid (MMA), dimethylarsinic acid (DMA), arsenobetaine (AsB), and arsenocholine (AsC)] in sea mustard (Undaria pinnatifida), dashima (Laminaria japonica), and laver (Porphyra tenera) of seaweed. After extraction under sonication with a solution of 50%(v/v) methanol in 1% HNO3 and subsequent clean-up with anion-exchange cartridge, arsenic species were quantified by liquid chromatography with inductively coupled plasma-mass spectrometry. The ion-exchange cartridge is effective to remove a lot of interference. The gradient elution method was used for high resolution of arsenic species and the optimum pH of mobile phase is 6.0 and 6.2. Limit of detection and quantification were set at 0.06–0.12 and 0.20–0.40 ng/mL, respectively. Overall recoveries of arsenic species from fortified samples in seaweed were 81.1–118.8%, except for AsB and AsC in dashima and laver. This proposed method could be useful for quantification and speciation of arsenic species in seaweed as well as other foodstuffs. |
| Starting Page | 39 |
| Ending Page | 44 |
| Page Count | 6 |
| File Format | |
| ISSN | 12267708 |
| Journal | Food Science and Biotechnology |
| Volume Number | 20 |
| Issue Number | 1 |
| e-ISSN | 20926456 |
| Language | English |
| Publisher | The Korean Society of Food Science and Technology |
| Publisher Date | 2011-02-28 |
| Publisher Place | Heidelberg |
| Access Restriction | One Nation One Subscription (ONOS) |
| Subject Keyword | arsenic speciation seaweed clean-up Nutrition Food Science |
| Content Type | Text |
| Resource Type | Article |
| Subject | Applied Microbiology and Biotechnology Food Science Biotechnology |
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