NDLI: EQCM studies of composition and electrochemical performance of film prepared by electrochemical reduction of sodium ferrate

Content Provider	Springer Nature Link
Author	Zhao, Li Chen, Bai Shuang Zhang, Jia Lin Wang, Dian Long
Copyright Year	2011
Abstract	A solid film was prepared by electrodepositing on a gold-film-coated quartz crystal electrode in Na2FeO4 solution, and characterized in 1 M LiClO4/propylene carbonate (PC) + 1, 2-dimethoxyethane (DME; 1:1 by volume) electrolyte using electrochemical quartz crystal microbalance (EQCM). The EQCM experimental and X-ray photoelectron spectroscopy results indicate that the composition of the electrodeposited solid film prepared in the potential range of 0.18 to −0.57 V vs. Ag/AgCl is FeOOH; and almost 1 mol lithium ions can be intercalated into and then extracted from 1 mol FeOOH film during discharge/charge process in 1 M LiClO4/PC + DME electrolyte. The discharge/charge experiment indicates that the specific capacity of FeOOH film stabilizes at a value close to its theoretical specific capacity after 20 cycles, and FeOOH film maintains a specific capacity of about 300 mAh g−1 at the end of 170 cycles. It is therefore concluded that the FeOOH film has a good electrochemical cycle ability in 1 M LiClO4/PC + DME electrolyte.
Starting Page	2079
Ending Page	2084
Page Count	6
File Format	PDF
ISSN	14328488
Journal	Journal of Solid State Electrochemistry
Volume Number	16
Issue Number	6
e-ISSN	14330768
Language	English
Publisher	Springer-Verlag
Publisher Date	2011-12-25
Publisher Place	Berlin, Heidelberg
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	Electrochemical quartz crystal microbalance Ferrate Film electrode Lithium ion battery Analytical Chemistry Condensed Matter Physics Characterization and Evaluation of Materials Electrochemistry Energy Storage Physical Chemistry
Content Type	Text
Resource Type	Article
Subject	Condensed Matter Physics Materials Science Electrical and Electronic Engineering Electrochemistry

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