NDLI: Certification of the mass fractions of Pt, Pd and Rh in a used car catalyst reference material

Content Provider	Springer Nature Link
Author	Recknagel, S. Michaelis, M.
Copyright Year	2009
Abstract	The high economic value of catalysts containing the platinum group elements platinum, rhodium and palladium as active components causes the need to be able to measure the precious metal loading with small uncertainty and to have suitable certified reference materials fulfilling high demands on the quality of the certified values. In European Reference Material ERM®-EB504, a used cordierite-based car catalyst material, mass fractions of platinum, palladium and rhodium were certified. The raw material was milled, homogenised and annealed before analysis. Seventeen laboratories experienced in precious metals analysis participated in the certification interlaboratory comparison, most of them analysing with inductively coupled plasma optical emission spectrometry using different sample pretreatment techniques. Homogeneity testing was carried out using X-ray fluorescence spectrometry. The certified mass fractions of Pt, Pd and Rh and their expanded uncertainties (k = 2) in ERM®-EB504 are (1777 ± 15), (279 ± 6) and (338 ± 4) mg/kg respectively.
Starting Page	277
Ending Page	280
Page Count	4
File Format	PDF
ISSN	09491775
Journal	Accreditation and Quality Assurance
Volume Number	14
Issue Number	5
e-ISSN	14320517
Language	English
Publisher	Springer-Verlag
Publisher Date	2009-03-19
Publisher Place	Berlin, Heidelberg
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	Precious metals CRM European reference material Platinum Rhodium Palladium ICP OES Marketing Ecotoxicology Biochemistry Analytical Chemistry Commercial Law Food Science
Content Type	Text
Resource Type	Article
Subject	Chemistry Instrumentation Chemical Engineering Safety, Risk, Reliability and Quality

Sl.	Authority	Responsibilities	Communication Details
1	Ministry of Education (GoI), Department of Higher Education	Sanctioning Authority	https://www.education.gov.in/ict-initiatives
2	Indian Institute of Technology Kharagpur	Host Institute of the Project: The host institute of the project is responsible for providing infrastructure support and hosting the project	https://www.iitkgp.ac.in
3	National Digital Library of India Office, Indian Institute of Technology Kharagpur	The administrative and infrastructural headquarters of the project	Dr. B. Sutradhar bsutra@ndl.gov.in
4	Project PI / Joint PI	Principal Investigator and Joint Principal Investigators of the project	Dr. B. Sutradhar bsutra@ndl.gov.in Prof. Saswat Chakrabarti will be added soon
5	Website/Portal (Helpdesk)	Queries regarding NDLI and its services	support@ndl.gov.in
6	Contents and Copyright Issues	Queries related to content curation and copyright issues	content@ndl.gov.in
7	National Digital Library of India Club (NDLI Club)	Queries related to NDLI Club formation, support, user awareness program, seminar/symposium, collaboration, social media, promotion, and outreach	clubsupport@ndl.gov.in
8	Digital Preservation Centre (DPC)	Assistance with digitizing and archiving copyright-free printed books	dpc@ndl.gov.in
9	IDR Setup or Support	Queries related to establishment and support of Institutional Digital Repository (IDR) and IDR workshops	idr@ndl.gov.in

A novel flow-injection method for simultaneous measurement of platinum (Pt), palladium (Pd) and rhodium (Rh) in aqueous soil extracts of contaminated soil by ICP-OES

Certification of the mass fractions of trace elements and pentachlorophenol in an impregnated wood reference material

ETV-ICP-OES: a useful technique for homogeneity study of trace element in metals—application to the homogeneity study of 23 elements in electrolytic copper

Assessment of the determination of heavy metals in organic soil improvers by ICP–OES

Determination of platinum, palladium and rhodium in Pt-catalysts by high performance thin layer chromatography using densitometry

The Use of Dowex-M43 Ion-exchange Resin in the Determination of Pt and Pd in Converter Matte by ICP-OES

Preparation and certification of a reference material for the total mercury and methylmercury mass fractions in fish

Certification of reference materials for ochratoxin A analysis in coffee and wine

Use of ETAAS, FAAS and ICP-OES for production and post-certification monitoring of a multielemental certified reference material according to national regulation limits for elements in drinking water

Certification of the mass fractions of Pt, Pd and Rh in a used car catalyst reference material

Similar Documents

A novel flow-injection method for simultaneous measurement of platinum (Pt), palladium (Pd) and rhodium (Rh) in aqueous soil extracts of contaminated soil by ICP-OES

Certification of the mass fractions of trace elements and pentachlorophenol in an impregnated wood reference material

ETV-ICP-OES: a useful technique for homogeneity study of trace element in metals—application to the homogeneity study of 23 elements in electrolytic copper

Assessment of the determination of heavy metals in organic soil improvers by ICP–OES

Determination of platinum, palladium and rhodium in Pt-catalysts by high performance thin layer chromatography using densitometry

The Use of Dowex-M43 Ion-exchange Resin in the Determination of Pt and Pd in Converter Matte by ICP-OES

Preparation and certification of a reference material for the total mercury and methylmercury mass fractions in fish

Certification of reference materials for ochratoxin A analysis in coffee and wine

Use of ETAAS, FAAS and ICP-OES for production and post-certification monitoring of a multielemental certified reference material according to national regulation limits for elements in drinking water

Certification of the mass fractions of Pt, Pd and Rh in a used car catalyst reference material