NDLI: Mass spectrometric analysis of ceramic components for solid oxide fuel cells

Content Provider	Springer Nature Link
Author	Becker, Johanna Sabine Westheide, Jochen Saprykin, Anatolij I. Holzbrecher, Horst Breuer, Uwe Dietze, Hans Joachim
Copyright Year	1997
Abstract	For the determination of trace impurities in ceramic components of solid oxide fuel cells (SOFCs), some mass spectrometric methods have been applied such as spark source mass spectrometry (SSMS), laser ionization mass spectrometry (LIMS), laser ablation inductively coupled plasma mass spectrometry (LA-ICP-MS) and inductively coupled plasma mass spectrometry (ICP-MS). Due to a lack of suitable standard reference materials for quantifying of analytical results on La x Sr y MnO3 cathode material a matrix-matched synthetic standard-high purity initial compounds doped with trace elements-was prepared in order to determine the relative sensitivity coefficients in SSMS and LA-ICP-MS. Radiofrequency glow discharge mass spectrometry (rf-GDMS) was developed for trace analysis and depth profiling of thick non-conducting layers. Surface analytical techniques, such as secondary ion mass spectrometry (SIMS) and sputtered neutral mass spectrometry (SNMS), were used to determine the element distribution on surfaces (homogeneity) and the surface contaminants of SOFC ceramic layers.
Starting Page	153
Ending Page	160
Page Count	8
File Format	PDF
ISSN	00263672
Journal	Microchimica Acta
Volume Number	125
Issue Number	1-4
e-ISSN	14365073
Language	English
Publisher	Springer-Verlag
Publisher Date	1997-01-01
Publisher Place	Vienna
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	mass spectrometry solid oxide fuel cells trace analysis Analytical Chemistry Inorganic Chemistry Physical Chemistry Characterization and Evaluation Materials Monitoring/Environmental Analysis/Environmental Ecotoxicology
Content Type	Text
Resource Type	Article
Subject	Analytical Chemistry

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