NDLI: Dispersive solid phase extraction of lead(II) using a silica nanoparticle-based ionic liquid ferrofluid

Content Provider	Springer Nature Link
Author	Fasih Ramandi, Negin Shemirani, Farzaneh Davudabadi Farahani, Malihe
Copyright Year	2014
Abstract	We demonstrate the application of an ionic liquid-based ferrofluid to the dispersive solid phase extraction of lead(II) using PAN as the chelator. The ionic liquid contains silica nanoparticles with a magnetic core as the dispersion medium, and its use results in improved stability of the colloidal dispersion and a complete extraction of lead(II) within a few seconds. In addition, there is no need for centrifugation. Specifically, the effect of different variables on the extraction of lead(II) was studied using an experimental design. Lead(II) was quantified by AAS. Under optimized conditions, the calibration graph for lead(II) is linear in the range from 5 to 372 μg L−1, the relative standard deviation is 1.34 % (for n = 7), the limit of detection is 1.66 μg L−1, and the enrichment factor is 200. The maximum adsorption capacity of sorbent was calculated to be 10.7 mg g−1, and adsorption follows a Langmuir isotherm. Figure A schematic view of D-SPE experimental set up. We demonstrate the application of an ionic liquid-based ferrofluid to the dispersive solid phase extraction of lead(II) using PAN as the chelator. The ionic liquid contains silica nanoparticles with a magnetic core as the dispersion medium
Starting Page	1833
Ending Page	1841
Page Count	9
File Format	PDF
ISSN	00263672
Journal	Microchimica Acta
Volume Number	181
Issue Number	15-16
e-ISSN	14365073
Language	English
Publisher	Springer Vienna
Publisher Date	2014-04-24
Publisher Place	Vienna
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	Ionic liquid-based ferrofluids Dispersive solid phase extraction Magnetic nanoparticles Ionic liquid- based ferrofluid Central composite design Nanochemistry Nanotechnology Characterization and Evaluation of Materials Analytical Chemistry Microengineering
Content Type	Text
Resource Type	Article
Subject	Analytical Chemistry

Sl.	Authority	Responsibilities	Communication Details
1	Ministry of Education (GoI), Department of Higher Education	Sanctioning Authority	https://www.education.gov.in/ict-initiatives
2	Indian Institute of Technology Kharagpur	Host Institute of the Project: The host institute of the project is responsible for providing infrastructure support and hosting the project	https://www.iitkgp.ac.in
3	National Digital Library of India Office, Indian Institute of Technology Kharagpur	The administrative and infrastructural headquarters of the project	Dr. B. Sutradhar bsutra@ndl.gov.in
4	Project PI / Joint PI	Principal Investigator and Joint Principal Investigators of the project	Dr. B. Sutradhar bsutra@ndl.gov.in Prof. Saswat Chakrabarti will be added soon
5	Website/Portal (Helpdesk)	Queries regarding NDLI and its services	support@ndl.gov.in
6	Contents and Copyright Issues	Queries related to content curation and copyright issues	content@ndl.gov.in
7	National Digital Library of India Club (NDLI Club)	Queries related to NDLI Club formation, support, user awareness program, seminar/symposium, collaboration, social media, promotion, and outreach	clubsupport@ndl.gov.in
8	Digital Preservation Centre (DPC)	Assistance with digitizing and archiving copyright-free printed books	dpc@ndl.gov.in
9	IDR Setup or Support	Queries related to establishment and support of Institutional Digital Repository (IDR) and IDR workshops	idr@ndl.gov.in

Magnetic silica nanomaterials for solid-phase extraction combined with dispersive liquid-liquid microextraction of ultra-trace quantities of plasticizers

Dispersive solid phase extraction of lead(II) using a silica nanoparticle-based ionic liquid ferrofluid

Fabrication of Fe3O4@graphene oxide core-shell nanospheres for ferrofluid-based dispersive solid phase extraction as exemplified for Cd(II) as a model analyte

Solid phase ligand-less extraction of cadmium(II) using a silica gel modified with an amino-functionalized ionic liquid

Oleate functionalized magnetic nanoparticles as sorbent for the analysis of polychlorinated biphenyls in juices

Supported hydrophobic ionic liquid on magnetic nanoparticles as a new sorbent for separation and preconcentration of lead and cadmium in milk and water samples

Surfactant-enhanced liquid-liquid microextraction coupled to micro-solid phase extraction onto highly hydrophobic magnetic nanoparticles

Silica-coated Mn3O4 nanoparticles coated with an ionic liquid for use in solid phase extraction of silver(I) ions prior to their determination by AAS

A three phase dispersive liquid-liquid microextraction technique for the extraction of antibiotics in milk

Dispersive solid phase extraction of lead(II) using a silica nanoparticle-based ionic liquid ferrofluid

Similar Documents

Magnetic silica nanomaterials for solid-phase extraction combined with dispersive liquid-liquid microextraction of ultra-trace quantities of plasticizers

Dispersive solid phase extraction of lead(II) using a silica nanoparticle-based ionic liquid ferrofluid

Fabrication of Fe3O4@graphene oxide core-shell nanospheres for ferrofluid-based dispersive solid phase extraction as exemplified for Cd(II) as a model analyte

Solid phase ligand-less extraction of cadmium(II) using a silica gel modified with an amino-functionalized ionic liquid

Oleate functionalized magnetic nanoparticles as sorbent for the analysis of polychlorinated biphenyls in juices

Supported hydrophobic ionic liquid on magnetic nanoparticles as a new sorbent for separation and preconcentration of lead and cadmium in milk and water samples

Surfactant-enhanced liquid-liquid microextraction coupled to micro-solid phase extraction onto highly hydrophobic magnetic nanoparticles

Silica-coated Mn3O4 nanoparticles coated with an ionic liquid for use in solid phase extraction of silver(I) ions prior to their determination by AAS

A three phase dispersive liquid-liquid microextraction technique for the extraction of antibiotics in milk

Dispersive solid phase extraction of lead(II) using a silica nanoparticle-based ionic liquid ferrofluid