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Membrane electrochemical reactors (MER) for NADH regeneration in HLADH-catalysed synthesis: comparison of effectiveness

Content Provider	Springer Nature Link
Author	Délécouls Servat, K. Bergel, A. Basséguy, R.
Copyright Year	2004
Abstract	Two membrane electrochemical reactors (MER) were designed and applied to HLADH-catalysed reduction of cyclohexanone to cyclohexanol. The regeneration of the cofactor NADH was ensured electrochemically, using either methyl viologen or a rhodium complex as electrochemical mediator. A semi-permeable membrane (dialysis or ultra-filtration) was integrated in the filter-press electrochemical reactor to confine the enzyme(s) as close as possible to the electrode surface. When methyl viologen was used, the transformation ratio of cyclohexanone varied from 0 to 65% depending on the internal arrangement of the reactor. Matching the reactor configuration to the reaction system was essential in this case. With the rhodium complex, the ultra-filtration MER was tested in continuous and recycling configurations. The best conditions led to 100% transformation of 0.1 L volume of 0.1 M cyclohexanone after 70 h with the recycling mode. Finally, the performances of the reactors are discussed with respect to different evaluations of the production yields.
Starting Page	205
Ending Page	215
Page Count	11
File Format	PDF
ISSN	16157591
Journal	Bioprocess Engineering
Volume Number	26
Issue Number	4
e-ISSN	16157605
Language	English
Publisher	Springer-Verlag
Publisher Date	2004-04-01
Publisher Place	Berlin, Heidelberg
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	Electrochemistry Enzyme catalysis Membranes Electrochemical reactor Synthesis
Content Type	Text
Resource Type	Article
Subject	Medicine Bioengineering Biotechnology

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