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| Content Provider | Springer Nature Link |
|---|---|
| Author | Liao, Xiaojuan Zhang, Hailiang Chen, Jianfang Wang, Xiayu |
| Copyright Year | 2006 |
| Abstract | A series of novel miktoarm star polymers composed of a poly(ethylene oxide) (PEO) and two side-chain liquid crystalline azobenzene-containing polymethacrylate (PEO-(PMMAZO)2) were prepared using atom transfer radical polymerization (ATRP). Bifunctional macroinitiator PEO-Br2 was synthesized by condensation reaction in two steps and characterized by 1H NMR, 13C NMR and IR. Kinetic study showed that it was a first order reaction referred to the monomer MMAZO, namely, 6-(4-methoxy-4’-oxy-azobenzene)hexyl methacrylate. The liquid crystalline behaviors of the miktoarm star polymers were studied by differential scanning calorimetry (DSC) and polarized optical microscope (POM). They exhibited smectic and nematic mesophases when Mn was beyond 9.4×103 g/mol. The phase transition temperatures of the smectic and nematic phases increased while the melting temperature of PEO decreased with increasing molecular weight of the LC block. Compared with diblock polymer PEO-PMMAZO, the melting temperature of PEO in miktoarm star polymer decreased more rapidly. |
| Starting Page | 819 |
| Ending Page | 828 |
| Page Count | 10 |
| File Format | |
| ISSN | 01700839 |
| Journal | Polymer Bulletin |
| Volume Number | 58 |
| Issue Number | 5-6 |
| e-ISSN | 14362449 |
| Language | English |
| Publisher | Springer-Verlag |
| Publisher Date | 2006-12-23 |
| Publisher Place | Berlin, Heidelberg |
| Access Restriction | One Nation One Subscription (ONOS) |
| Subject Keyword | Polymer Sciences Characterization and Evaluation of Materials Soft Matter, Complex Fluids Physical Chemistry |
| Content Type | Text |
| Resource Type | Article |
| Subject | Chemistry Materials Chemistry Condensed Matter Physics Polymers and Plastics |
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