NDLI: Preparation and characterization of thermally stable poly(amide–ester–imide) nanocomposites based on N,N′-(1,3,5,7-tetraoxo-5,7-dihydropyrrolo [3,4-f]isoindole-2,6-(1H,3H)-diyl)bis-(4-hydroxybenzamide) and surface-coated TiO2 nanoparticles

Content Provider	Springer Nature Link
Author	Mallakpour, Shadpour Aalizadeh, Roghayeh
Copyright Year	2016
Abstract	A thermally stable and optically active poly(amide–ester–imide) (PAEI) was prepared from diol: N,N′-(1,3,5,7-tetraoxo-5,7-dihydropyrrolo[3,4-f]isoindole-2,6-(1H,3H)-diyl)bis-(4-hydroxybenzamide). The structure of the polymer was determined by means of 1H NMR and Fourier transform infrared spectroscopy (FT-IR), elemental analysis; also it was studied with specific rotation technique, X-ray diffraction (XRD), and field emission scanning electron microscopy (FE-SEM). Then, three series of PAEI/modified TiO2 nanocomposites (NC)s with 5, 10, and 15 % of TiO2 nanoparticles (NP)s contents were prepared via ultrasonic irradiation technique. The properties of the synthesized NCs were studied by FT-IR, XRD, FE-SEM, transmission electron microscopy, UV–vis spectroscopy and thermogravimetric analysis methods. It was found that the NCs exhibit enhanced thermal properties compared with the neat PAEI.
Starting Page	3019
Ending Page	3032
Page Count	14
File Format	PDF
ISSN	01700839
Journal	Polymer Bulletin
Volume Number	73
Issue Number	11
e-ISSN	14362449
Language	English
Publisher	Springer Berlin Heidelberg
Publisher Date	2016-03-16
Publisher Place	Berlin, Heidelberg
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	Poly(amide–ester–imide) Organomodified TiO2 nanoparticle Nanocomposite Thermal stability Polymer Sciences Soft and Granular Matter, Complex Fluids and Microfluidics Characterization and Evaluation of Materials Physical Chemistry
Content Type	Text
Resource Type	Article
Subject	Chemistry Materials Chemistry Condensed Matter Physics Polymers and Plastics

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3,3′-(1,3,5,7-Tetraoxo-2,3,6,7-tetrahydro-1H,5H-pyrrolo[3,4-f]isoindole-2,6-diyl)dipropanoic acid N,N-dimethylformamide disolvate

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