NDLI: Determination of Cyantraniliprole and its Major Metabolite Residues in Pakchoi and Soil Using Ultra-Performance Liquid Chromatography

Content Provider	Springer Nature Link
Author	Sun, Jianpeng Feng, Nan Tang, Congfeng Qin, Dongmei
Copyright Year	2012
Abstract	A rapid, simple and reliable analytical method was developed for the determination of cyantraniliprole and its major metabolite J9Z38 in pakchoi and soil by using ultra-performance liquid chromatography–tandem mass spectrometry (UPLC–MS/MS). The sample preparation approach is known as QuEChERS, which stands for quick, easy, cheap, effective, rugged and safe. Samples were extracted with acetonitrile, and cleaned up with dispersive primary and secondary amine sorbent before analysis by UPLC–MS/MS. The limit of quantitation for cyantraniliprole and J9Z38 was 0.01 mg/kg in both pakchoi and soil. Average recoveries of cyantraniliprole and J9Z38 at three fortified levels (0.01, 0.05, 0.1 mg/kg) ranged from 77.8 % to 102.5 % with relative standard deviation of 1.6 %–8.9 %. This method has been applied to the analysis of cyantraniliprole and J9Z38 residues in real pakchoi and soil samples selected from field. The results of the residue dynamic experiment showed that the half-life of cyantraniliprole ranged from 2.9 to 6.4 days in pakchoi and 8.7 to 18.2 days in soil, respectively. The final residual levels of cyantraniliprole in pakchoi and soil from Guangdong and Shanghai were below 0.20 and 0.10 mg/kg, respectively; similarly, the final residual levels of J9Z38 in pakchoi and soil from Guangdong and Shanghai were <0.07 and 0.01 mg/kg. These results will be helpful in setting maximum residue limit guidance for cyantraniliprole in pakchoi in China.
Starting Page	845
Ending Page	852
Page Count	8
File Format	PDF
ISSN	00074861
Journal	Bulletin of Environmental Contamination and Toxicology
Volume Number	89
Issue Number	4
e-ISSN	14320800
Language	English
Publisher	Springer-Verlag
Publisher Date	2012-08-30
Publisher Place	New York
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	Cyantraniliprole J9Z38 UPLC–MS/MS Residue Pakchoi Environmental Chemistry Ecotoxicology Waste Water Technology / Water Pollution Control / Water Management / Aquatic Pollution Environmental Health Soil Science & Conservation Pollution
Content Type	Text
Resource Type	Article
Subject	Health, Toxicology and Mutagenesis Pollution Medicine Toxicology

Sl.	Authority	Responsibilities	Communication Details
1	Ministry of Education (GoI), Department of Higher Education	Sanctioning Authority	https://www.education.gov.in/ict-initiatives
2	Indian Institute of Technology Kharagpur	Host Institute of the Project: The host institute of the project is responsible for providing infrastructure support and hosting the project	https://www.iitkgp.ac.in
3	National Digital Library of India Office, Indian Institute of Technology Kharagpur	The administrative and infrastructural headquarters of the project	Dr. B. Sutradhar bsutra@ndl.gov.in
4	Project PI / Joint PI	Principal Investigator and Joint Principal Investigators of the project	Dr. B. Sutradhar bsutra@ndl.gov.in Prof. Saswat Chakrabarti will be added soon
5	Website/Portal (Helpdesk)	Queries regarding NDLI and its services	support@ndl.gov.in
6	Contents and Copyright Issues	Queries related to content curation and copyright issues	content@ndl.gov.in
7	National Digital Library of India Club (NDLI Club)	Queries related to NDLI Club formation, support, user awareness program, seminar/symposium, collaboration, social media, promotion, and outreach	clubsupport@ndl.gov.in
8	Digital Preservation Centre (DPC)	Assistance with digitizing and archiving copyright-free printed books	dpc@ndl.gov.in
9	IDR Setup or Support	Queries related to establishment and support of Institutional Digital Repository (IDR) and IDR workshops	idr@ndl.gov.in

Determination of Residual Flubendiamide in the Cabbage by QuEChERS-Liquid Chromatography–Tandem Mass Spectrometry

Residues and Dynamics of Kasugamycin in Chilli and Soil

Determination of Residues of Fipronil and Its Metabolites in Cauliflower by Using Gas Chromatography-Tandem Mass Spectrometry

Ultra-high performance liquid chromatography-electrospray tandem mass spectrometry for the analysis of antibiotic residues in environmental waters

Determination of 4,4′-, 3,4′-, and 2,2′-Diaminodiphenylethers in Sediment Samples from the Sea Using Liquid Chromatography-Tandem Mass Spectrometry

Determination of Trenbolone Residual in Bovine Liver by Liquid Chromatography–Mass Spectrometry

Facile and Rapid Determination of Contamination in Sulphur Pesticide Formulations by Liquid Chromatography–Tandem Mass Spectrometry

Determination of N,N-Dimethyldodecylamine and N,N-Dimethyloctadecylamine in River and Sea Water Using Liquid Chromatography Tandem Mass Spectrometry

Dissipation and Residue Determination of Fluoroglycofen-Ethyl in Soybean and Soil by UPLC-MS–MS

Determination of Cyantraniliprole and its Major Metabolite Residues in Pakchoi and Soil Using Ultra-Performance Liquid Chromatography–Tandem Mass Spectrometry

Similar Documents

Determination of Residual Flubendiamide in the Cabbage by QuEChERS-Liquid Chromatography–Tandem Mass Spectrometry

Residues and Dynamics of Kasugamycin in Chilli and Soil

Determination of Residues of Fipronil and Its Metabolites in Cauliflower by Using Gas Chromatography-Tandem Mass Spectrometry

Ultra-high performance liquid chromatography-electrospray tandem mass spectrometry for the analysis of antibiotic residues in environmental waters

Determination of 4,4′-, 3,4′-, and 2,2′-Diaminodiphenylethers in Sediment Samples from the Sea Using Liquid Chromatography-Tandem Mass Spectrometry

Determination of Trenbolone Residual in Bovine Liver by Liquid Chromatography–Mass Spectrometry

Facile and Rapid Determination of Contamination in Sulphur Pesticide Formulations by Liquid Chromatography–Tandem Mass Spectrometry

Determination of N,N-Dimethyldodecylamine and N,N-Dimethyloctadecylamine in River and Sea Water Using Liquid Chromatography Tandem Mass Spectrometry

Dissipation and Residue Determination of Fluoroglycofen-Ethyl in Soybean and Soil by UPLC-MS–MS

Determination of Cyantraniliprole and its Major Metabolite Residues in Pakchoi and Soil Using Ultra-Performance Liquid Chromatography–Tandem Mass Spectrometry