NDLI: Simultaneous Determination of Spinetoram Residues in Tomato by High Performance Liquid Chromatography Combined with QuEChERS Method

Content Provider	Springer Nature Link
Author	Malhat, Farag Mahmoud
Copyright Year	2012
Abstract	A sensitive and simple method for simultaneous analysis of spinetoram residues and its dissipation in tomato were studied. Spinetoram residues were extracted from tomato samples with acetonitrile. The extract was cleaned-up with QuEChERS method by dispersive solid-phase extraction with primary secondary amine sorbent to remove co-extractives, prior to analysis by high performance liquid chromatography coupled with diode array detector (HPLC–DAD). This method is characterized by recovery >97 %, relative standard division (RSD) <12.3 %, and limit of quantification (LOQ) of 0.04 mg kg−1, in agreement with directive for method validation in residue analysis. Also, the results showed that spinetoram dissipation pattern followed the first order kinetics with the half-life of 2.6 days, in tomato. The spinetoram residues in tomato were below the codex maximum residue level (0.06 mg kg−1) after 10 days of application. This study suggests that spinetoram is acceptable to apply for tomato under the recommended dosage.
Starting Page	222
Ending Page	226
Page Count	5
File Format	PDF
ISSN	00074861
Journal	Bulletin of Environmental Contamination and Toxicology
Volume Number	90
Issue Number	2
e-ISSN	14320800
Language	English
Publisher	Springer-Verlag
Publisher Date	2012-11-15
Publisher Place	New York
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	Spinetoram Residue Dissipation HPLC–DAD Pollution Environmental Health Ecotoxicology Soil Science & Conservation Environmental Chemistry Waste Water Technology / Water Pollution Control / Water Management / Aquatic Pollution
Content Type	Text
Resource Type	Article
Subject	Health, Toxicology and Mutagenesis Pollution Medicine Toxicology

Sl.	Authority	Responsibilities	Communication Details
1	Ministry of Education (GoI), Department of Higher Education	Sanctioning Authority	https://www.education.gov.in/ict-initiatives
2	Indian Institute of Technology Kharagpur	Host Institute of the Project: The host institute of the project is responsible for providing infrastructure support and hosting the project	https://www.iitkgp.ac.in
3	National Digital Library of India Office, Indian Institute of Technology Kharagpur	The administrative and infrastructural headquarters of the project	Dr. B. Sutradhar bsutra@ndl.gov.in
4	Project PI / Joint PI	Principal Investigator and Joint Principal Investigators of the project	Dr. B. Sutradhar bsutra@ndl.gov.in Prof. Saswat Chakrabarti will be added soon
5	Website/Portal (Helpdesk)	Queries regarding NDLI and its services	support@ndl.gov.in
6	Contents and Copyright Issues	Queries related to content curation and copyright issues	content@ndl.gov.in
7	National Digital Library of India Club (NDLI Club)	Queries related to NDLI Club formation, support, user awareness program, seminar/symposium, collaboration, social media, promotion, and outreach	clubsupport@ndl.gov.in
8	Digital Preservation Centre (DPC)	Assistance with digitizing and archiving copyright-free printed books	dpc@ndl.gov.in
9	IDR Setup or Support	Queries related to establishment and support of Institutional Digital Repository (IDR) and IDR workshops	idr@ndl.gov.in

Estimation of Etofenprox Residues in Tomato Fruits by QuEChERS Methodology and HPLC–DAD

Residue and Dissipation Dynamics of Lufenuron in Tomato Fruit Using QuEChERS Methodology

Dissipation and Residue Determination of Ningnanmycin in Cucumber and Soil by High Performance Liquid Chromatography with Ultraviolet Detector

Simultaneous Determination of Flubendiamide its Metabolite Desiodo Flubendiamide Residues in Cabbage, Tomato and Pigeon Pea by HPLC

Determination of Bromothalonil Residues and Degradation in Apple and Soil by QuEChERS and GC–MS/MS

Determination of Diacylhydrazines-Type Insect Growth Regulator JS-118 Residues in Cabbage and Soil by High Performance Liquid Chromatography with DAD Detection

Determination of Oxadiargyl Residues in Environmental Samples and Rice Samples

Dissipation of Hexythiozox on Beans Pods by HPLC–DAD

Dissipation Rate and Residue Distribution of Dufulin in Tomato and Soil Under Field Conditions

Simultaneous Determination of Spinetoram Residues in Tomato by High Performance Liquid Chromatography Combined with QuEChERS Method

Similar Documents

Estimation of Etofenprox Residues in Tomato Fruits by QuEChERS Methodology and HPLC–DAD

Residue and Dissipation Dynamics of Lufenuron in Tomato Fruit Using QuEChERS Methodology

Dissipation and Residue Determination of Ningnanmycin in Cucumber and Soil by High Performance Liquid Chromatography with Ultraviolet Detector

Simultaneous Determination of Flubendiamide its Metabolite Desiodo Flubendiamide Residues in Cabbage, Tomato and Pigeon Pea by HPLC

Determination of Bromothalonil Residues and Degradation in Apple and Soil by QuEChERS and GC–MS/MS

Determination of Diacylhydrazines-Type Insect Growth Regulator JS-118 Residues in Cabbage and Soil by High Performance Liquid Chromatography with DAD Detection

Determination of Oxadiargyl Residues in Environmental Samples and Rice Samples

Dissipation of Hexythiozox on Beans Pods by HPLC–DAD

Dissipation Rate and Residue Distribution of Dufulin in Tomato and Soil Under Field Conditions

Simultaneous Determination of Spinetoram Residues in Tomato by High Performance Liquid Chromatography Combined with QuEChERS Method