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Optimized Synthesis of Di, Tri and Tetrafused Pyridazinium Cations
| Content Provider | Semantic Scholar |
|---|---|
| Author | Siro, Jorge G. Ramos, Andrés Vaquero, Juan J. Alvarez-Builla, Julio G. Garcı́a-Navı́o, J. Luis |
| Copyright Year | 2000 |
| Abstract | Abstract By combining two complementary statistical techniques (fractional factorial experimental design and simplex operation) the synthesis of the parent pyrido[1,2- b ]-pyridazinium cation has been successfully carried out (the yield was improved from less than 10 to 65%) by basic condensation of 2-methyl-1-aminopyridinium mesitylenesulfonate and [1,4]dioxane-2,3-diol. Using the optimized reaction conditions, other related heterocyclic cations could be prepared, and two interesting examples are now reported. |
| Starting Page | 2469 |
| Ending Page | 2472 |
| Page Count | 4 |
| File Format | PDF HTM / HTML |
| DOI | 10.1016/S0040-4020(00)00079-X |
| Alternate Webpage(s) | http://dspace.uah.es/dspace/bitstream/handle/10017/4192/art.pdf;jsessionid=86782C19525854605A496A0F814966B2?sequence=1 |
| Alternate Webpage(s) | https://doi.org/10.1016/S0040-4020%2800%2900079-X |
| Volume Number | 56 |
| Language | English |
| Access Restriction | Open |
| Content Type | Text |
| Resource Type | Article |