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Determination of volatile residual solvents in pharmaceutical products by headspace liquid-phase microextraction gas chromatography-flame ionization detector
| Content Provider | Semantic Scholar |
|---|---|
| Author | Wang, Xia Jiang, Ting Yuan, Jinpeng Cheng, Chuange Liu, Jianhua Shi, Junbo Zhao, Ru-Song |
| Copyright Year | 2006 |
| Abstract | This paper demonstrates headspace liquid-phase microextraction (HS-LPME) as used for the determination of volatile residual solvents in pharmaceutical products. This method is based on headspace liquid-phase microextraction capillary column gas chromatography. Under optimum conditions, the linerary of the method ranged from 1 to 1,000 mg l−1. The limits of detection are 0.2–2.0 mg l−1 and relative standard deviations (RSD) for most of the volatile solvents were below 10%. This novel method is applied to the analysis of volatile residual solvents in pharmaceutical products with satisfactory results. |
| Starting Page | 1082 |
| Ending Page | 1086 |
| Page Count | 5 |
| File Format | PDF HTM / HTML |
| DOI | 10.1007/s00216-006-0506-2 |
| Alternate Webpage(s) | https://rd.springer.com/content/pdf/10.1007/s00216-006-0506-2.pdf |
| PubMed reference number | 16770579 |
| Alternate Webpage(s) | https://doi.org/10.1007/s00216-006-0506-2 |
| Journal | Medline |
| Volume Number | 385 |
| Journal | Analytical and bioanalytical chemistry |
| Language | English |
| Access Restriction | Open |
| Content Type | Text |
| Resource Type | Article |
