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Darstellung und Charakterisierung von Bis(η5-1,2,3,4,5-Pentamethylcyclo-pentadienyl)(η3-1-phenylallyl)lanthanum˙Tetrahydrofuran
| Content Provider | Semantic Scholar |
|---|---|
| Author | Kretschmer, Winfried P. Brummelhuis, Bas Ten Meetsma, Auke Teuben, Jan H. |
| Copyright Year | 2006 |
| Abstract | The title compound has been prepared from Cp-2*LaCl2K(THF)(2) and 1-PhC3H4K-(THF)(0.5) in THF suspension, forming yellow single crystals from hexane solution which were characterized in solid state and in solution by elementary analysis, IR, C-13- and variable temperature H-1-NMR spectroscopy and a crystal structure determination. Space group P1, Z = 2, T = 130 K, a = 8.595(1), b = 10.770(1), c = 17.903(5) angstrom, alpha = 93.54(1)degrees, beta = 98.30(1)degrees, gamma = 112.42(1)degrees, R = 0.0249. |
| Starting Page | 1933 |
| Ending Page | 1935 |
| Page Count | 3 |
| File Format | PDF HTM / HTML |
| DOI | 10.1002/zaac.200600141 |
| Volume Number | 632 |
| Alternate Webpage(s) | https://www.rug.nl/research/portal/files/6699098/2006ZAnorgAllgChemKretschmerT.pdf |
| Alternate Webpage(s) | https://doi.org/10.1002/zaac.200600141 |
| Language | English |
| Access Restriction | Open |
| Content Type | Text |
| Resource Type | Article |