NDLI: A multiresidue method for the determination of abamectin, doramectin, moxidectin, ivermectin, milbemectin A(3), and milbemectin A(4) residues in bovine muscle using HPLC with fluorescence detection

Please wait, while we are loading the content...

A multiresidue method for the determination of abamectin, doramectin, moxidectin, ivermectin, milbemectin A(3), and milbemectin A(4) residues in bovine muscle using HPLC with fluorescence detection

Content Provider	Semantic Scholar
Author	Chou, Hsien-Hsin Lai, Chun Yuen. Chen, Tie Hong Yen, Gow Chin 顏國欽
Copyright Year	2003
Abstract	Abamectin, doramectin, moxidectin, ivermectin, milbemectin A 3 and milbemectin A4 are similar macrocyclic lactone chemicals used as parasiticides or acaricides. A method using high performance liquid chromatography (HPLC) with fluorescence detection is presented for the simultaneous determination of the residue amounts of these compounds in bovine muscle. Samples are extracted using acetonitrile and cleaned up with solid phase extraction using a C18 column, followed by fluorescence-derivatized with 1-methyli midazole and trifluoroacetic anhydride in acetonitrile. The analogue was measured by HPLC with fluorescence detector at 365 nm exc itation and 470 nm emission wavelengths. The limits of quantification are below the stipulated Taiwan Maximum Residue Limit for e ach compound. The recoveries of this method in bovine muscle ranged from 73.3 to 110%, with a RSD from 2.11 to 16.57%. The detection limit of those 6 compounds in bovine muscle was 5 ppb. No any above compounds were detected in 50 samples of bovine muscle tested. Therefore, the developed method can be used for rapid screen of macrocyclic lactones in bovine muscle.
File Format	PDF HTM / HTML
Alternate Webpage(s)	http://www.fda.gov.tw/tc/includes/GetFile.ashx?chk=36409bb4-caf4-4e77-b3b6-623c36ab9fe2&id=8349&mID=148
Language	English
Access Restriction	Open
Content Type	Text
Resource Type	Article

Sl.	Authority	Responsibilities	Communication Details
1	Ministry of Education (GoI), Department of Higher Education	Sanctioning Authority	https://www.education.gov.in/ict-initiatives
2	Indian Institute of Technology Kharagpur	Host Institute of the Project: The host institute of the project is responsible for providing infrastructure support and hosting the project	https://www.iitkgp.ac.in
3	National Digital Library of India Office, Indian Institute of Technology Kharagpur	The administrative and infrastructural headquarters of the project	Dr. B. Sutradhar bsutra@ndl.gov.in
4	Project PI / Joint PI	Principal Investigator and Joint Principal Investigators of the project	Dr. B. Sutradhar bsutra@ndl.gov.in Prof. Saswat Chakrabarti will be added soon
5	Website/Portal (Helpdesk)	Queries regarding NDLI and its services	support@ndl.gov.in
6	Contents and Copyright Issues	Queries related to content curation and copyright issues	content@ndl.gov.in
7	National Digital Library of India Club (NDLI Club)	Queries related to NDLI Club formation, support, user awareness program, seminar/symposium, collaboration, social media, promotion, and outreach	clubsupport@ndl.gov.in
8	Digital Preservation Centre (DPC)	Assistance with digitizing and archiving copyright-free printed books	dpc@ndl.gov.in
9	IDR Setup or Support	Queries related to establishment and support of Institutional Digital Repository (IDR) and IDR workshops	idr@ndl.gov.in