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Determination of hydroxylated polycyclic aromatic hydrocarbons in airborne particulates by high-performance liquid chromatography with fluorescence detection.
| Content Provider | Semantic Scholar |
|---|---|
| Author | Kishikawa, Naoya Morita, Seigo Wada, Mitsuhiro Ohba, Yoshihito Nakashima, Kenichiro Kuroda, Naotaka |
| Copyright Year | 2004 |
| Abstract | This paper describes a highly sensitive and selective method for the determination of hydroxylated polycyclic aromatic hydrocarbons (PAHs-OH) in airborne particulates. PAHs-OH were extracted from airborne particulates with ethanol by ultrasonication. The extractant was further cleaned up by solid phase extraction (SPE) with an aminopropylsilica cartridge, and subsequently analyzed by reversed-phase high-performance liquid chromatography with fluorescence detection. 2-Hydroxy-1-acetonaphthone was used as an internal standard. By the proposed method, 2-hydroxyfluorene and 1-hydroxypyrene were identified in airborne particulates and their concentrations were determined for the first time. |
| Starting Page | 195 |
| Ending Page | 201 |
| Page Count | 7 |
| File Format | PDF HTM / HTML |
| Alternate Webpage(s) | https://www.jstage.jst.go.jp/article/analsci/20/1/20_1_129/_pdf/-char/en |
| PubMed reference number | 14753270v1 |
| Volume Number | 20 |
| Issue Number | 1 |
| Journal | Analytical sciences : the international journal of the Japan Society for Analytical Chemistry |
| Language | English |
| Access Restriction | Open |
| Subject Keyword | 1-hydroxypyrene 2-hydroxyfluorene 2-nitrophenylhydrazine AROMATICS Cleaning (activity) Ethanol Fluorescence Hydrocarbons Hydroxyl Radical Liquid Chromatography Particulate (substance) Polycyclic Hydrocarbons, Aromatic Solid Phase Extraction |
| Content Type | Text |
| Resource Type | Article |
