NDLI: Azidation of β-keto esters and silyl enol ethers with a benziodoxole reagent.

Content Provider	Semantic Scholar
Author	Vita, Maria Victoria Waser, Jérôme
Copyright Year	2013
Abstract	The efficient azidation of β-keto esters and silyl enol ethers using a benziodoxole-derived azide transfer reagent is reported. The azidation of cyclic β-keto esters could be achieved in up to quantitative yields in the absence of any catalyst. In the case of less reactive linear β-keto esters and silyl enol ethers, complete conversion and good yields could be obtained by using a zinc catalyst.
Starting Page	36
Ending Page	37
Page Count	2
File Format	PDF HTM / HTML
Alternate Webpage(s)	https://infoscience.epfl.ch/record/189470/files/OL2013-3246GreenAccess.pdf
PubMed reference number	23773166v1
Alternate Webpage(s)	https://doi.org/10.1021/ol401229v
DOI	10.1021/ol401229v
Journal	Organic letters
Volume Number	15
Issue Number	13
Language	English
Access Restriction	Open
Subject Keyword	3-oxoadipate enol-lactonase activity Azides Brominated Diphenyl Ethers Carnitine esters:SCnt:Pt:Tiss:Qn Crown Ethers Cyclic GMP Esters Ethers for general anesthesia Reagents benziodoxole enol
Content Type	Text
Resource Type	Article

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Azidation of β-keto esters and silyl enol ethers with a benziodoxole reagent.