NDLI: Kristallstruktur von 1,1'-Dimethyl-4,4'-bipyridinium-octachlorodiantimonat(III) / Crystal Structure of 1,1'-Dimethyl-4,4'-bipyridinium-octachlorodiantimonate(III)

Content Provider	Semantic Scholar
Author	Jaschinski, B. Blachnik, Roger Reuter, Hans
Copyright Year	1998
Abstract	Abstract The title compound was prepared by reaction of SbCl3 with 1,1′-dimethyl-4,4′-bipyridinium-chloride in methanol. The single crystal structure gave the following data: [C12H14N2][Sb2Cl8] (1) space group PI, Nr. 1, with a = 570.68(7) pm, b = 938.57(14) pm, c = 1174.27(11)pm, α = 66.72(9)°, β = 89.304(12)°, γ = 78.684(11)°, and Z = 1. The compound has a small SHG effect and a phase transition at 272 °C with an enthalpy of transition of 6.54 kJ mol-1 .
Starting Page	565
Ending Page	568
Page Count	4
File Format	PDF HTM / HTML
DOI	10.1515/znb-1998-5-613
Alternate Webpage(s)	http://www.znaturforsch.com/ab/v53b/53b0565.pdf
Alternate Webpage(s)	http://zfn.mpdl.mpg.de/data/Reihe_B/53/ZNB-1998-53b-0565.pdf
Alternate Webpage(s)	https://doi.org/10.1515/znb-1998-5-613
Volume Number	53
Language	English
Access Restriction	Open
Content Type	Text
Resource Type	Article

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