NDLI: Regioselective Reaction of Heterocyclic N-Oxides, an Acyl Chloride, and Cyclic Thioethers.

Content Provider	Semantic Scholar
Author	Frei, Przemyslaw Jones, Douglas H. Kay, Steven T. McLellan, Jayde A. Johnston, Blair F. Kennedy, Alan R. Tomkinson, Nicholas C. O.
Copyright Year	2018
Abstract	Treatment of electron deficient pyridine N-oxides with 4-nitrobenzoyl chloride and a cyclic thioether in the presence of triethylamine leads to the corresponding 2-functionalized product in up to a 74% isolated yield. The transformation can also be accomplished with alternative nitrogen containing heterocycles, including quinolines, pyrimidines, and pyrazines. To expand the scope of the transformation, diisopropyl ether can be used as the reaction medium to allow for the use of solid thioether substrates.
Starting Page	1510
Ending Page	1517
Page Count	8
File Format	PDF HTM / HTML
DOI	10.1021/acs.joc.7b02457
PubMed reference number	29345136
Journal	Medline
Volume Number	83
Issue Number	3
Alternate Webpage(s)	https://strathprints.strath.ac.uk/63045/1/Frei_etal_JOC2018_Regioselective_reaction_of_heterocyclic_N_oxides_an_acyl_chloride.pdf
Alternate Webpage(s)	https://doi.org/10.1021/acs.joc.7b02457
Journal	The Journal of organic chemistry
Language	English
Access Restriction	Open
Content Type	Text
Resource Type	Article

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