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Direct incorporation of vanadium into three-dimensional KIT-6: 1. Optimization of synthesis conditions
| Content Provider | Semantic Scholar |
|---|---|
| Author | Jermy, Balasamy Rabindran Kim, Sang-Yun Bineesh, Kanattukara Vijayan Selvaraj, Manickam Park, Dae-Won |
| Copyright Year | 2009 |
| Abstract | Three dimensional (3-D) cubic KIT-6 with directly incorporated vanadium was hydrothermally synthesized by using Pluronic P123 and n-butanol as the structure-directing mixture, tetraethyl orthosilicate (TEOS) as the silica source and NH4VO3 as the vanadium source. The molar composition was varied in the range of 0.017 P123/0.08–2.4 V/1.0–2.0 TEOS/1.31–1.70 BuOH/1.83–3.00 HCl/195 H2O. The orderness of mesopore structure was estimated by X-ray diffraction, N2 adsorption, and TEM analysis. The effects of the amount of HCl, TEOS and BuOH on the structure of KIT-6 were discussed. The time and temperature for the synthesis of KIT-6 were also optimized. The amount of vanadium content influenced the framework structure and crystallinity of the Ia3d phase significantly. |
| Starting Page | 1235 |
| Ending Page | 1240 |
| Page Count | 6 |
| File Format | PDF HTM / HTML |
| DOI | 10.1007/s11814-009-0199-2 |
| Alternate Webpage(s) | https://page-one.springer.com/pdf/preview/10.1007/s11814-009-0199-2 |
| Alternate Webpage(s) | https://www.cheric.org/PDF/KJChE/KC26/KC26-5-1235.pdf |
| Alternate Webpage(s) | https://doi.org/10.1007/s11814-009-0199-2 |
| Volume Number | 26 |
| Language | English |
| Access Restriction | Open |
| Content Type | Text |
| Resource Type | Article |
