NDLI: Determination of polycyclic aromatic hydrocarbons in honey by matrix solid-phase dispersion and gas chromatography/mass spectrometry.

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Determination of polycyclic aromatic hydrocarbons in honey by matrix solid-phase dispersion and gas chromatography/mass spectrometry.

Content Provider	Semantic Scholar
Author	Albero, Beatriz Sánchez-Brunete, Consuelo Tadeo, José L.
Copyright Year	2003
Abstract	A multiresidue method was developed for the de termination of 16 polycyclic aromatic hydrocarbons (PAHs) in unifloral and multifloral honeys. The analytical procedure is based on the matrix solid-phase dispersion of honey on a mixture of Florisil and anhydrous sodium sulfate in small glass columns and extraction with hexane-ethyl acetate (90 + 10, v/v) with assisted sonication. The PAH residues are determined by gas chromatography with mass spectrometric detection using selected-ion monitoring. Average recoveries for all the PAHs studied were in the range of almost 80 to 101%, with relative standard deviations of 6 to 15%. The limits of detection ranged from 0.04 to 2.9 microg/kg. The simultaneous extraction and cleanup of samples makes this method simple and rapid, with low consumption of organic solvents
File Format	PDF HTM / HTML
DOI	10.1093/jaoac/86.3.576
Alternate Webpage(s)	http://lib3.dss.go.th/fulltext/Journal/J.AOAC%201999-2003/J.AOAC2003/v86n3(may-jun)/v86n3p576.pdf
PubMed reference number	12852579
Alternate Webpage(s)	https://doi.org/10.1093/jaoac%2F86.3.576
Journal	Medline
Volume Number	86
Issue Number	3
Journal	Journal of AOAC International
Language	English
Access Restriction	Open
Content Type	Text
Resource Type	Article

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