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[Evaluation of method for simultaneous determination of pesticide residues in fruits and vegetables by collaborative study].
| Content Provider | Semantic Scholar |
|---|---|
| Author | Kakimoto, Yoshihisa Naetoko, Yoshitaka Hara, Hiroyuki Miyatake, Makoto Sato, Arata Tatsuguchi, Hisako Takahata, Ryoichi Yamamoto, Ryosuke Joh, Teruo |
| Copyright Year | 2004 |
| Abstract | A collaborative study involving 8 laboratories was conducted to evaluate a method for the simultaneous determination of pesticide residues in 6 types of fruits and vegetables (spinach, tomato, apple, radish, cabbage and carrot). The method of analysis was the same as reported by Kakimoto et al. in 2003. One hundred and thirty-nine pesticides were spiked by each of 8 laboratories at levels of 0.1 microg/g (pesticides analyzed by GC/MS) or 0.5 microg/g (pesticides analyzed by HPLC) into the 6 kinds of samples. Statistical analysis showed that 111 pesticides could be analyzed with practical precision by this method. For screening purposes, the method could analyze 118 pesticides. The median values of the limits of detection were 0.001-0.041 microg/g. The calibration curves were linear in the range of 0.5-5 microg/mL for most pesticides with median correlation coefficients of 0.983-1.000. |
| Starting Page | 075701 |
| Ending Page | 075701 |
| Page Count | 1 |
| File Format | PDF HTM / HTML |
| Alternate Webpage(s) | https://www.jstage.jst.go.jp/article/shokueishi/45/3/45_3_165/_pdf/-char/ja |
| PubMed reference number | 15468938v1 |
| Volume Number | 45 |
| Issue Number | 3 |
| Journal | Shokuhin eiseigaku zasshi. Journal of the Food Hygienic Society of Japan |
| Language | English |
| Access Restriction | Open |
| Subject Keyword | Brassica oleracea Calibration Fruit High pressure liquid chromatography procedure Laboratory Pesticide Residues Pesticides Spinach - dietary Thirty Nine Vegetables |
| Content Type | Text |
| Resource Type | Article |
