NDLI: Synthesis and crystal structure of an iron(II) dimeric complex

Content Provider	Semantic Scholar
Author	Roy, Partha Pratim Dhara, Koushik Chakraborty, Jishnunil Nethaji, Munirathinam Banerjee, Pradyot
Copyright Year	2007
Abstract	An iron(II) complex, $[Fe_2(salen)_2]$ has been prepared by the reaction of $[Fe^{III}(salen)Cl]$ with copper(II) malonate dihydrate [salen = N,N'-ethylenebis(salicylideneiminato) dianion] in N,N-dimethylformamide-water mixture. The complex has been characterized by FT-IR spectroscopy, UV-vis spectra, thermogravimetric analysis, cyclic voltammetry and X-ray crystallography. The iron(II) complex 1 crystallizes in the monoclinic, space group C2/c, a = 26.664(5) \AA, b = 6.9943(11) \AA, c = 14.727(2) \AA, $\beta = 97.498(3)^o$, and Z = 8. The structural study reveals that it is a penta-coordinate Fe(II) dimeric complex.
Starting Page	1947
Ending Page	1950
Page Count	4
File Format	PDF HTM / HTML
Volume Number	46
Alternate Webpage(s)	http://nopr.niscair.res.in/bitstream/123456789/2219/1/IJCA%2046A(12)%201947-1950.pdf
Language	English
Access Restriction	Open
Content Type	Text
Resource Type	Article

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