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Synthesis and Spectral Studies of Zn II , Cd II and Hg II Complexes with 5-( 2-Benzoic acid azo )-8-hydroxy quinoline Ligand
| Content Provider | Semantic Scholar |
|---|---|
| Author | Jarad, Amer J. Kadhim, Muna A. Jabrallah, Shahryar A. |
| Copyright Year | 2015 |
| Abstract | Coupling reaction of 2-amino benzoic acid with 8-hydroxy quinoline gave bidentate azo ligand. The prepared ligand has been identified by Microelemental Analysis, 1 HNMR,FT-IR and UV-Vis spectroscopic techniques. Treatment of the prepared ligand with the following metal ions (Zn II ,Cd II and Hg II ) in aqueous ethanol with a 1:2 M:L ratio and at optimum pH, yielded a series of neutral complexes of the general formula [M(L)2]. The prepared complexes have been characterized by using flame atomic absorption, (C.H.N) Analysis, FT-IR and UV-Vis spectroscopic methods as well as conductivity measurements. The nature of the complexes formed were studied following the mole ratio and continuous variation methods, Beer's law obeyed over a concentration range (1× 10 -4 3 × 10 -4 M). High molar absorbtivity of the complex solutions have been observed. The stability constant of the complexes has also been studied. |
| File Format | PDF HTM / HTML |
| Alternate Webpage(s) | https://www.iasj.net/iasj?aId=24285&func=fulltext |
| Language | English |
| Access Restriction | Open |
| Content Type | Text |
| Resource Type | Article |
