NDLI: Elucidating the elusive crystal structure of 2,4,6-tris(2-pyrimidyl)-1,3,5-triazine

Content Provider	Semantic Scholar
Author	Safin, Damir A. Tumanov, Nikolay A. Leitch, Alicea A. Brusso, Jaclyn L. Filinchuk, Yaroslav Murugesu, Muralee
Copyright Year	2015
Abstract	2,4,6-Tris(2-pyrimidyl)-1,3,5-triazine (TPymT) has been synthesized using two approaches: via trimerization of 2-cyanopyrimidine at 160 °C and by the reaction of 2-cyanopyrimidine with pyrimidine-2-carboximidamide. It was found that the two different synthetic pathways to TPymT yielded either a single polymorph or a mixture of two polymorphs; both of which were studied for the first time by X-ray powder diffraction (XRPD) and synchrotron X-ray powder diffraction (SXRPD). The crystal structure of the polymorph α-TPymT was determined by single crystal X-ray diffraction (SCXRD). Crystal structures of 2-cyanopyrimidine and pyrimidine-2-carboximidamide were also elucidated by SXRPD.
Starting Page	2190
Ending Page	2195
Page Count	6
File Format	PDF HTM / HTML
DOI	10.1039/C5CE00097A
Volume Number	17
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Alternate Webpage(s)	http://mysite.science.uottawa.ca/mmuruges/publications/2015/Safin_CrystEngComm_2015_c5ce00097a.pdf
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Alternate Webpage(s)	https://doi.org/10.1039/C5CE00097A
Language	English
Access Restriction	Open
Content Type	Text
Resource Type	Article

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