NDLI: Reduction of Polyfunctional Aromatic Nitro Compounds Using Lithium Aluminum Hydride.

Content Provider	Semantic Scholar
Author	Joseph, Manu M. Jacob, Dominic
Copyright Year	2004
Abstract	Aromatic nitro compounds containing yet another functional group are reduced using lithium aluminium hydride in ether. The reduction of nitrobenzanilides results in preferential reduction of amide functionality while the isomeric N- (nitrophenyl) benzamides results in preferential cleavage of the amide bond. Besides, the reduction of 2,2'-dinitrodiphenyl amine 5a, reduction of (bis-2-nitroanilino) methane 5b, 2, 2'-dinitrodiphenylether 5c, 2-nitrophenyl-2'-nitrophenoxymethane 5d, 1, 3-dinitrobenzene 6a, 2-nitrobenzaldoxime 6b, 2-N (2'-nitrophenylmethyl) amino benzoic acid 6c, 2-nitrophenoxymethyl phenyl ketone 6d are carried out. Nitro group is found reluctant towards reduction in some cases whereas in some others it is reduced into different extents. This points to the limitation of the suggested azo test for aromatic nitro compounds.
Starting Page	432
Ending Page	436
Page Count	5
File Format	PDF HTM / HTML
DOI	10.1002/chin.200422059
Volume Number	35
Alternate Webpage(s)	http://nopr.niscair.res.in/bitstream/123456789/18748/1/IJCB%2043B(2)%20432-436.pdf
Alternate Webpage(s)	https://doi.org/10.1002/chin.200422059
Language	English
Access Restriction	Open
Content Type	Text
Resource Type	Article

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