NDLI: Large-scale and local-scale structures in polymer-blend films: a grazing-incidence ultra-small-angle X-ray scattering and sub-microbeam grazing-incidence small-angle X-ray scattering investigation

Content Provider	Semantic Scholar
Author	Müller-Buschbaum, Peter Bauer, Estelle Maurer, Eugen Roth, Stephan V. Gehrke, Rainer Burghammer, Manfred Riekel, Christian
Copyright Year	2006
Abstract	Phase-separation structures are installed by solution casting and flow of a binary polymer-blend solution of polystyrene and poly-n-butylacrylate in toluene on silicon. Optical microscopy and scanning-probe microscopy measurements provide the surface topography. Large-scale structures are probed with high-resolution or grazing-incidence ultra-small-angle X-ray scattering enabled by high reciprocal-space resolution. Correspondingly, structures of up to 13 µm are resolved. Local-scale structures are detected with sub-microbeam grazing-incidence small-angle X-ray scattering, providing a high real-space resolution of 1 µm. Nanometre-size cavities are found in the polystyrene-rich parts of the blend film.
File Format	PDF HTM / HTML
DOI	10.1107/S0021889806048369
Volume Number	40
Alternate Webpage(s)	http://journals.iucr.org/j/issues/2007/s1/00/aj6011/aj6011.pdf
Alternate Webpage(s)	https://doi.org/10.1107/S0021889806048369
Language	English
Access Restriction	Open
Content Type	Text
Resource Type	Article

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