NDLI: Synthesis and characterization of nano silicon and titanium nitride powders using atmospheric microwave plasma technique

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Synthesis and characterization of nano silicon and titanium nitride powders using atmospheric microwave plasma technique

Content Provider	Semantic Scholar
Author	Kumar, S. Murugan, Karuppiah Chandrasekhar, S. Hebalkar, Neha Krishna, Murali Satyanarayana, B. Madras, Giridhar
Copyright Year	2012
Abstract	AbstractWe have demonstrated a simple, scalable and inexpensive method based on microwave plasma for synthesizing 5 to 10 g/h of nanomaterials. Luminescent nano silicon particles were synthesized by homogenous nucleation of silicon vapour produced by the radial injection of silicon tetrachloride vapour and nano titanium nitride was synthesized by using liquid titanium tetrachloride as the precursor. The synthesized nano silicon and titanium nitride powders were characterized by XRD, XPS, TEM, SEM and BET. The characterization techniques indicated that the synthesized powders were indeed crystalline nanomaterials. Graphical AbstractA simple, scalable and inexpensive method based on microwave plasma was developed for synthesizing 5 to 10 g/h of silicon and titanium nitride nanopowders. Silicon was synthesized by homogenous nucleation of silicon vapour while titanium nitride was synthesized by using liquid titanium tetrachloride as the precursor.
Starting Page	557
Ending Page	563
Page Count	7
File Format	PDF HTM / HTML
DOI	10.1007/s12039-012-0256-y
Alternate Webpage(s)	https://www.ias.ac.in/article/fulltext/jcsc/124/03/0557-0563
Alternate Webpage(s)	https://doi.org/10.1007/s12039-012-0256-y
Volume Number	124
Journal	Journal of Chemical Sciences
Language	English
Access Restriction	Open
Content Type	Text
Resource Type	Article

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