NDLI: Peptide synthesis using novel S-sulfocysteine derivatives

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Peptide synthesis using novel S-sulfocysteine derivatives

Content Provider	Scilit
Author	Maugras, Isabelle Gosteli, Jacques Rapp, Elke Nyfeler, Rolf
Copyright Year	2009
Description	Journal: International journal of peptide and protein research New cysteine S-sulfonate derivatives, Boc-Cys(SO3Na)-ONa 2 and Fmoc-Cys(SO3Na)-ONa 3, were prepared and their utility for peptide synthesis examined. The Fmoc derivative 3 was used in the solid-phase peptide synthesis of Arg8-vasopressin 9 via the Bunte salt 7. Satisfactory S-sulfonate stability was observed when p-cresol scavenged the cleavage from the resin. The intermediate 7 was purified by ion-exchange chromatography prior to S-sulfonate cleavage with tributylphosphine.
Related Links	http://onlinelibrary.wiley.com/doi/10.1111/j.1399-3011.1995.tb01034.x/pdf
Ending Page	156
Page Count	5
Starting Page	152
ISSN	03678377
DOI	10.1111/j.1399-3011.1995.tb01034.x
Journal	International journal of peptide and protein research
Issue Number	2
Volume Number	45
Language	English
Publisher	Wiley-Blackwell
Publisher Date	2009-01-12
Access Restriction	Open
Subject Keyword	Journal: International journal of peptide and protein research Medicinal Chemistry Organic Chemistry Cysteine Side‐chain Protecting Group Solid‐phase Peptide Synthesis
Content Type	Text
Resource Type	Article
Subject	Biochemistry

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