NDLI: Síntese da fenitoína assistida por micro-ondas: proposta de aula prática para alunos de graduação

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Síntese da fenitoína assistida por micro-ondas: proposta de aula prática para alunos de graduação

Content Provider	Scilit
Author	Konrath, Eduardo L. Piedade, Maristela Eifler-Lima, Vera Lucia
Copyright Year	2012
Description	Microwave synthesis is considered a breakthrough in the field of chemistry due to its benefits over conventional heating methods. We describe, for the first time, the total synthesis of phenytoin adapted for a microwave reactor, proposed as an experiment for undergraduate courses. When carried out with microwaves, the synthetic route provided phenytoin in 6 min and 30 s, while for conventional heating the total time was 170 min. The experiment also involves rapid identification of compounds by TLC, ¹H NMR, FT-IR and melting points determination
Related Links	http://www.scielo.br/scielo.php?script=sci_pdf&pid=S0100-40422012000900033&lng=pt&nrm=iso&tlng=en
Ending Page	1890
Page Count	4
Starting Page	1887
ISSN	01004042
e-ISSN	01004042
DOI	10.1590/s0100-40422012000900033
Journal	Química Nova
Issue Number	9
Volume Number	35
Language	English
Publisher	FapUNIFESP (SciELO)
Publisher Date	2012-01-01
Access Restriction	Open
Subject Keyword	Química Nova Sntese Da Da Fenitona Fenitona Assistida Micro Ondas Assistida Por Por Micro Prtica Para
Content Type	Text
Resource Type	Article
Subject	Chemistry

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