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Synthesis and characterization carboxyl functionalized Multi-Walled Carbon Nanotubes (MWCNT-COOH) and $NH_{2}$ functionalized Multi-Walled Carbon Nanotubes $(MWCNTNH_{2}$)
| Content Provider | Scilit |
|---|---|
| Author | Arifin Wulandari, S. A. Widiyandari, Hendri Subagio, Agus |
| Copyright Year | 2018 |
| Description | Journal: Journal of Physics: Conference Series A making of MWCNTs-COOH has been conducted to improve the compatibility of carbon nanotubes and $MWCNTs-NH_{2}$, in order to have conductive properties. The MWCNTs- COOH study was performed, using the first reflux method using $HNO_{3}$ for 6 hours heated with 60°C (concentrated $HNO_{3}$ ratio with MWCNTs is 1: 5), followed by the second reflux using $SOCl_{2}$ for 5 hours heated to 70°C (concentrated $HNO_{3}$ ratio with MWCNTs is 1: 3). Meanwhile, the making of $MWCNTs-NH_{2}$ used homogenization process, used magnetic stirrer, with comparison between MWCNTs-COOH with Etanadiamine 1: 2000, for 8 hours at 40oC. Both products were analyzed using Fourier transform infrared (FTIR), Scanning Electron Microscopy (SEM) and Energy Dispersive X-Ray Spectroscopy (EDS). The C-O bond on MWCNTs-COOH is indicated by absorption at wavelength 1672.28 $cm^{-1}$ and O-H bond at 3431.36 $cm^{-1}$ N-H bond on $MWCNTs-NH_{2}$ shown at wavelength 1440.83. The SEM analysis indicates that both products have a tubular surface morphology. |
| Related Links | https://iopscience.iop.org/article/10.1088/1742-6596/1025/1/012005/pdf http://iopscience.iop.org/article/10.1088/1742-6596/1025/1/012005/pdf |
| ISSN | 17426588 |
| e-ISSN | 17426596 |
| DOI | 10.1088/1742-6596/1025/1/012005 |
| Journal | Journal of Physics: Conference Series |
| Issue Number | 1 |
| Volume Number | 1025 |
| Language | English |
| Publisher | IOP Publishing |
| Publisher Date | 2018-05-30 |
| Access Restriction | Open |
| Subject Keyword | Journal: Journal of Physics: Conference Series |
| Content Type | Text |
| Resource Type | Article |
| Subject | Physics and Astronomy |