NDLI: Preparation and characterization of aminosilane-functionalized cellulose nanocrystal aerogel

Please wait, while we are loading the content...

Preparation and characterization of aminosilane-functionalized cellulose nanocrystal aerogel

Content Provider	Scilit
Author	Wu, Yu Cao, Fei Jiang, Hua Zhang, Yang
Copyright Year	2017
Description	Journal: Materials Research Express In this study, cellulose nanocrystal (CNC) extracted from hybrid poplar residue was grafted with an aminosilane, N-(2-aminoethyl)-3-aminopropylmethyldimethoxysilane (AEAPMDS). Supercritical $CO_{2}$ drying was employed to produce polymer aerogels. The effects of AEAPMDS on the properties of the aerogel were investigated. Fourier transform infrared spectroscopy confirmed that the aminosilane had been grafted on CNC. The crystallinity decreased due to the introduction of amorphous AEAPMDS on the surface of CNC. Analysis of specific surface areas and pore diameters indicated that the modification failed to destroy the inner structure of the aerogel. Scanning electron microscopy and thermogravimetry revealed that three-dimensional network structure was conserved after modification but had a lower thermal stability. High $CO_{2}$ adsorption capacities (1.7 and 2.6 mmol $g^{−1}$) were measured at 1 bar and two temperatures, 25 and 0 °C, respectively. Therefore, the modification procedure could be a promising avenue for the preparation of aminosilane-functionalized CNC aerogels as a novel adsorption material.
Related Links	http://iopscience.iop.org/article/10.1088/2053-1591/aa8067/pdf
ISSN	20531591
e-ISSN	20531591
DOI	10.1088/2053-1591/aa8067
Journal	Materials Research Express
Issue Number	8
Volume Number	4
Language	English
Publisher	IOP Publishing
Publisher Date	2017-08-01
Access Restriction	Open
Subject Keyword	Journal: Materials Research Express
Content Type	Text
Resource Type	Article
Subject	Surfaces, Coatings and Films Metals and Alloys Biomaterials Electronic, Optical and Magnetic Materials Polymers and Plastics

Central Library (ISO-9001:2015 Certified)
Indian Institute of Technology Kharagpur
Kharagpur, West Bengal, India | PIN - 721302

See location in the Map
03222 282435
Mail: support@ndl.gov.in

Sl.	Authority	Responsibilities	Communication Details
1	Ministry of Education (GoI), Department of Higher Education	Sanctioning Authority	https://www.education.gov.in/ict-initiatives
2	Indian Institute of Technology Kharagpur	Host Institute of the Project: The host institute of the project is responsible for providing infrastructure support and hosting the project	https://www.iitkgp.ac.in
3	National Digital Library of India Office, Indian Institute of Technology Kharagpur	The administrative and infrastructural headquarters of the project	Dr. B. Sutradhar bsutra@ndl.gov.in
4	Project PI / Joint PI	Principal Investigator and Joint Principal Investigators of the project	Dr. B. Sutradhar bsutra@ndl.gov.in Prof. Saswat Chakrabarti will be added soon
5	Website/Portal (Helpdesk)	Queries regarding NDLI and its services	support@ndl.gov.in
6	Contents and Copyright Issues	Queries related to content curation and copyright issues	content@ndl.gov.in
7	National Digital Library of India Club (NDLI Club)	Queries related to NDLI Club formation, support, user awareness program, seminar/symposium, collaboration, social media, promotion, and outreach	clubsupport@ndl.gov.in
8	Digital Preservation Centre (DPC)	Assistance with digitizing and archiving copyright-free printed books	dpc@ndl.gov.in
9	IDR Setup or Support	Queries related to establishment and support of Institutional Digital Repository (IDR) and IDR workshops	idr@ndl.gov.in